Skip to main content
Log in

Influence of Processing Severity During Equal-Channel Angular Pressing on the Microstructure of an Al-Zn-Mg-Cu Alloy

  • Published:
Metallurgical and Materials Transactions A Aims and scope Submit manuscript

Abstract

A commercial Al-Zn-Mg-Cu alloy, Al 7075, was overaged at 553 K (280 °C) for 5 hours and processed by equal-channel angular pressing (ECAP) using route BC. Different temperatures and number of passes, which determine the processing severity, were considered. The processing severity has been estimated by the maximum stress (σ Proc) recorded during each ECAP pass. The higher the number of passes or the lower the processing temperature, i.e., the higher is the processing severity, the finer the (sub)grain size is obtained. A minimum ultrafine (sub)grain size of approximately 150 nm after three passes at 353 K (80 °C) or eight passes at 403 K (130 °C) was obtained. The microhardness exhibited an instant increase from 76 HV for the overaged initial state to 115 HV after only the first pass. The coarsened precipitates in the overaged alloy lead to larger structural refinement than in pure aluminum.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11

Similar content being viewed by others

References

  1. J.E. Hatch, ed.: Aluminium: Properties and Physical Metallurgy, ASM, Materials Park, OH, 1984, p. 370.

  2. G. Fribourg, Y. Bréchet, J.L. Chemin, and A. Deschamps: Metall. Mater. Trans. A, 2011, in press.

  3. C.M. Cepeda-Jiménez, P. Hidalgo, M. Pozuelo, O.A. Ruano, and F. Carreño: Mater. Sci. Eng. A, 2010, vol. 527, pp. 2579–87.

    Article  Google Scholar 

  4. A.P. Zhilyaev, D.L. Swisher, K. Oh-ishi, T.G. Langdon, and T.R. McNelley: Mater. Sci. Eng. A, 2006, vol. 429, pp. 137–48.

    Article  Google Scholar 

  5. R.Z. Valiev, N.A. Krasilnikov, and N.K. Tsenev: Mater. Sci. Eng. A, 1991, vol. 137, pp. 35–40.

    Article  Google Scholar 

  6. R.Z. Valiev, R.R. Mulyukov, V.V. Ovchinnikov, and V.A. Shabashov: Scripta Metall. Mater., 1991, vol. 25, pp. 2717–22.

    Article  CAS  Google Scholar 

  7. N.A. Akhmadeev, N.P. Kobelev, R.R. Mulyukov, M.Y. Soifer, and R.Z. Valiev: Acta Metall. Mater., 1993, vol. 41, pp. 1041–46.

    Article  CAS  Google Scholar 

  8. S.D. Terhune, D.L. Swisher, K. Oh-Ishi, Z. Horita, T.G. Langdon, and T.R. McNelley: Metall. Mater. Trans. A, 2002, vol. 33A, pp. 2173–84.

    Article  CAS  Google Scholar 

  9. J.M. García-Infanta, S. Swaminathan, A.P. Zhilyaev, F. Carreño, O.A. Ruano, and T.R. McNelley: Mater. Sci. Eng. A, 2008, vol. 485, pp. 160–75.

    Article  Google Scholar 

  10. J.M. García-Infanta, S. Swaminathan, C.M. Cepeda-Jiménez, T.R. McNelley, O.A. Ruano, and F. Carreño: J. Alloys Compd., 2009, vol. 478, pp. 139–43.

    Article  Google Scholar 

  11. L. Balogh, R.B. Figueiredo, T. Ungár, and T.G. Langdon: Mater. Sci. Eng. A, 2010, vol. 528, pp. 533–38.

    Article  Google Scholar 

  12. V.M. Segal: Mater. Sci. Eng. A, 1995, vol. 197, pp. 157–64.

    Article  Google Scholar 

  13. T.G. Langdon: Rev. Metal. Madrid, 2008, vol. 44, pp. 556–64.

    CAS  Google Scholar 

  14. K. Oh-Ishi, Z. Horita, M. Furukawa, M. Nemoto, and T.G. Langdon: Metall. Mater. Trans. A, 1998, vol. 29A, pp. 2011–13.

    Article  CAS  Google Scholar 

  15. Y. Iwahashi, J. Wang, Z. Horita, M. Nemoto, and T.G. Langdon: Scripta Mater., 1996, vol. 35, pp. 143–46.

    Article  CAS  Google Scholar 

  16. Y. Iwahashi, Z. Horita, M. Nemoto, and T.G. Langdon: Acta Mater., 1998, vol. 46, pp. 3317–31.

    Article  CAS  Google Scholar 

  17. H. Kim, M. Soe, and S. Hong: Mater. Sci. Eng. A, 2000, vol. 291, pp. 86–90.

    Article  Google Scholar 

  18. T. Aida, K. Matsuki, Z. Horita, and T.G. Langdon: Scripta Mater., 2001, vol. 44, pp. 575–79.

    Article  CAS  Google Scholar 

  19. J. Suh, H. Kim, J. Park, and J. Chang: Scripta Mater., 2001, vol. 44, pp. 677–81.

    Article  CAS  Google Scholar 

  20. S.J. Oh and S.B. Kang: Mater. Sci. Eng. A, 2003, vol. 343, pp. 107–15.

    Article  Google Scholar 

  21. C. Xu and T.G. Langdon: Scripta Mater., 2003, vol. 48, pp. 1–4.

    Article  CAS  Google Scholar 

  22. D. Shin, D. Hwang, Y. Oh, and K. Park: Metall. Mater. Trans. A, 2004, vol. 35A, pp. 825–37.

    Article  CAS  Google Scholar 

  23. K. Turba, P. Málek, E.F. Rauch, and M. Cieslar: Mater. Sci. Forum, 2008, vols. 584–86, pp. 164–69.

  24. K. Turba, P. Málek, E.F. Rauch, F. Robaut, and M. Cieslar: Int. J. Mater. Res., 2009, vol. 100, pp. 851–57.

    Article  CAS  Google Scholar 

  25. Z.L. Ning, S. Guo, F.Y. Cao, G.J. Wang, Z.C. Li, and J.F. Sun: J. Mater. Sci., 2010, vol. 45, pp. 3023–29.

    Article  CAS  Google Scholar 

  26. L.J. Zheng, C.Q. Chen, T.T. Zhou, P.Y. Liu, and M.G. Zeng: Mater. Charact., 2002, vol. 49, pp. 455–61.

    Article  CAS  Google Scholar 

  27. C.Y. Nam, J.H. Han, Y.H. Chung, and M.C. Shin: Mater. Sci. Eng. A, 2003, vol. 347, pp. 253–57.

    Article  Google Scholar 

  28. Y.H. Zhao, X.Z. Liao, R.Z. Valiev, and Y.T. Zhu: Acta Mater., 2004, vol. 52, pp. 4589–99.

    Article  CAS  Google Scholar 

  29. P. Málek, M. Cieslar, and R.K. Islamgaliev: J. Alloys Compd., 2004, vol. 378, pp. 237–41.

    Article  Google Scholar 

  30. Y.H. Zhao, X.Z. Liao, R.Z. Valiev, and Y.T. Zhu: J. Mater. Res., 2005, vol. 20, pp. 288–91.

    Article  CAS  Google Scholar 

  31. G. Sha, Y.B. Wang, X.Z. Liao, Z.C. Duan, S.P. Ringer, and T.G. Langdon: Acta Mater., 2009, vol. 57, pp. 3123–32.

    Article  CAS  Google Scholar 

  32. Z.C. Duan, N.Q. Chinh, C. Xu, and T.G. Langdon: Metall. Mater. Trans. A, 2010, vol. 41A, pp. 802–09.

    Article  CAS  Google Scholar 

  33. S. Lee, A. Utsunomiya, H. Akamatsu, K. Neishi, M. Furukawa, Z. Horita, and T.G. Langdon: Acta Mater., 2003, vol. 50, pp. 553–64.

    Article  Google Scholar 

  34. C. Xu, M. Furukawa, Z. Horita, and T.G. Langdon: Acta Mater., 2003, vol. 51, pp. 6139–49.

    Article  CAS  Google Scholar 

  35. A. Momeni and K. Dehghani: Metall. Mater. Trans. A, 2011, vol. 42A, pp. 1925–32.

    Article  Google Scholar 

  36. M.Carsí, V. López, F. Peñalba, and O.A. Ruano: Mater. Sci. Eng. A, 1996, vol. 216, pp. 155–60.

    Article  Google Scholar 

  37. M. Eddahbi, J.A. Jiménez, and O.A. Ruano: J. Alloys Compd., 2007, vol. 433, pp. 97–107.

    Article  CAS  Google Scholar 

  38. J.A. Jiménez, M. Carsí, G. Frommeyer, S. Knippscher, J. Witting, and O.A. Ruano: Intermetallics, 2005, vol. 13, pp. 1021–29.

    Article  Google Scholar 

  39. P.J. Apps, M. Berta, and P.B. Prangnell: Acta Mater., 2005, vol. 53, pp. 499–511.

    Article  CAS  Google Scholar 

  40. P. Kumar, C. Xu, and T.G. Langdon: Mater. Sci. Eng. A, 2006, vol. 429, pp. 324–28.

    Article  Google Scholar 

  41. N. Kamikawa, X. Huang, N. Tsuji, and N. Hansen: Acta Mater., 2009, vol. 57, pp. 4198–4208.

    Article  CAS  Google Scholar 

  42. M.T. Pérez-Prado, J.A. del Valle, and O.A. Ruano: Scripta Mater., 2004, vol. 51, pp. 1093–97.

    Article  Google Scholar 

  43. A.P. Zhilyaev and T.G. Langdon: Progr. Mater. Sci., 2008, vol. 53, pp. 893–979.

    Article  CAS  Google Scholar 

  44. R.Z. Valiev and T.G. Langdon: Progr. Mater. Sci., 2006, vol. 51, pp. 881–981.

    Article  CAS  Google Scholar 

  45. O.D. Sherby and P.M. Burke: Progr. Mater. Sci., 1968, vol. 13, pp. 323–90.

    Article  Google Scholar 

  46. S. Komura, M. Furukawa, Z. Horita, M. Nemoto, and T.G. Langdon: Mater. Sci. Eng. A, 2001, vol. 297, pp. 111–18.

    Article  Google Scholar 

  47. G. Shigesato and E.F. Rauch: Mater. Sci. Eng. A, 2007, vol. 462, pp. 402–06.

    Article  Google Scholar 

  48. E.F. Rauch and M. Veron: Materialwissenschaft und Werkstofftechnick, 2005, vol. 36, pp. 552–56.

    Article  CAS  Google Scholar 

  49. E.R. Rauch and A. Duft: Mater. Sci. Forum, 2005, vols. 495–497, pp. 197–202.

  50. F.J. Humphreys and M. Hatherly: Recrystallization and Related Annealing Phenomenon, 2nd ed., Elsevier, Oxford, U.K., 2004, pp. 70–71.

    Google Scholar 

  51. J.A. Wert: Scripta Metall., 1981, vol. 15, pp. 445–47.

    Article  CAS  Google Scholar 

  52. R. Ayer, J.Y. Koo, J.W. Steeds, and B.K. Park: Metall. Trans. A, 1985, vol. 16A, pp. 1925–36.

    CAS  Google Scholar 

  53. R.Z. Valiev, R.K. Islamgaliev, N.F. Kuzmina, Y. Li, and T.G. Langdon: Scripta Mater., 1999, vol. 40, pp. 117–22.

    CAS  Google Scholar 

  54. A. Gholinia, P. Bate, and P.B. Prangnell: Acta Mater., 2002, vol. 50, pp. 2121–36.

    Article  CAS  Google Scholar 

  55. G.R. Canova, U.F. Kocks, and J.J. Jonas: Acta Metall., 1984, vol. 32, pp. 211–26.

    Article  CAS  Google Scholar 

  56. L.S. Tóth, R.A. Massion, L. Germain, S.C. Baik, and S. Suwas: Acta Mater., 2004, vol. 52, pp. 1885–98.

    Article  Google Scholar 

  57. E.A. El-Danaf: Mater. Sci. Eng. A, 2007, vol. 487, pp. 189–200.

    Google Scholar 

  58. T.R. McNelley and D.L. Swisher: TMS Symposium Ultrafine Grained Materials, vol. 3, Y.T. Zhu, T.G. Langdon, R.Z. Valiev, S.L. Semiatin, D.H. Shin, and T.C. Lowe, eds., 2004, pp. 89–94.

  59. J.C. Werenskiold and H.J. Roven: Mater. Sci. Eng. A, 2005, vols. 410–411, pp. 174–77.

    Google Scholar 

  60. C. Xu, M. Furukawa, Z. Horita, and T.G. Langdon: Mater. Sci. Eng. A, 2005, vol. 398, pp. 66–76.

    Article  Google Scholar 

  61. M. Murayama, Z. Horita, and K. Hono: Acta Mater., 2001, vol. 49, pp. 21–29.

    Article  CAS  Google Scholar 

  62. I. Gutierrez-Urrutia, M.A. Muñoz-Morris, and D.G. Morris: Mater. Sci. Eng. A, 2005, vol. 394, pp. 399–410.

    Article  Google Scholar 

  63. Z. Liu, S. Bai, X. Zhou, and Y. Gu: Mater. Sci. Eng. A, 2011, vol. 528, pp. 2217–22.

    Article  Google Scholar 

  64. K. Oh-Ishi, Y. Hashi, A. Sadakata, K. Kaneko, Z. Horita, and T.G. Langdon: Mater. Sci. Forum, 2002, vols. 396–402, pp. 333–38.

    Article  Google Scholar 

  65. G. Guiglionda and W.J. Poole: Mater. Sci. Eng. A, 2001, vols. 319–321, pp. 583–87.

    Google Scholar 

  66. A. Goloborodko, O. Sitdikov, R. Kaibyshev, H. Miura, and T. Sakai: Mater. Sci. Eng. A, 2004, vol. 381, pp. 121–28.

    Article  Google Scholar 

  67. H. Cao, J.Y. Min, S.D. Wu, A.P. Xian, and J.K. Shang: Mater. Sci. Eng. A, 2006, vol. 431, pp. 86–91.

    Article  Google Scholar 

  68. H.J. Roven, M. Liu, and J.C. Werenskiold: Mater. Sci. Eng. A, 2008, vols. 483–484, pp. 54–58.

    Google Scholar 

  69. P.B. Trivedi, R.S. Yassar, D.P. Field, and R. Alldredge: Mater. Sci. Eng. A, 2006, vol. 425, pp. 205–12.

    Article  Google Scholar 

  70. M.A. Muñoz-Morris, I. Gutierrez-Urrutia, and D.G. Morris: Mater. Sci. Eng. A, 2008, vol. 493, pp. 141–47.

    Article  Google Scholar 

  71. J. Zhang, N. Gao, and M.J. Starink: Mater. Sci. Eng. A, 2010, vol. 527, pp. 3472–79.

    Article  Google Scholar 

  72. O. Sitdikov, T. Sakai, H. Miura, and C. Hama: Mater. Sci. Eng. A, 2009, vol. 516, pp. 180–88.

    Article  Google Scholar 

  73. C.Y. Yu, P.L. Sun, P.W. Kao, and C.P. Chang: Mater. Sci. Eng. A, 2004, vol. 366, pp. 310–17.

    Article  Google Scholar 

  74. O. Sitdikov, T. Sakai, A. Goloborodko, H. Miura, and R. Kaibyshev: Philos. Mag., 2005, vol. 85, pp. 1159–75.

    Article  CAS  Google Scholar 

  75. C. Kobayashi, T. Sakai, A. Belyakov, and H. Miura: Philos. Mag. Lett., 2007, vol. 87, pp. 751–66.

    Article  CAS  Google Scholar 

  76. I. Mazurina, T. Sakai, H. Miura, O. Sitdikov, and R. Kaibyshev: Mater. Sci. Eng. A, 2008, vol. 473, pp. 297–305.

    Article  Google Scholar 

  77. T. Sakai, A. Belyakov, and H. Miura: Metall. Mater. Trans. A, 2008, vol. 39A, pp. 2206–14.

    Article  CAS  Google Scholar 

  78. I. Mazurina, T. Sakai, H. Miura, O. Sitdikov, and R. Kaibyshev: Metall. Mater. Trans., 2009, vol. 50, pp. 101–10.

    CAS  Google Scholar 

  79. S.N. Alhajeri, N. Gao, and T.G. Langdon: Mater. Sci. Eng. A, 2011, vol. 528, pp. 3833–40.

    Article  Google Scholar 

  80. Y. Iwahashi, Z. Horita, M. Nemoto, and T.G. Langdon: Metall. Mater. Trans. A, 1998, vol. 29A, pp. 2503–10.

    Article  CAS  Google Scholar 

  81. R. Roumina and C.W. Sinclair: Acta Mater., 2010, vol. 58, pp. 111–21.

    Article  CAS  Google Scholar 

  82. C. Xu, Z. Horita, and T.G. Langdon: Mater. Sci. Eng. A, 2011, vol. 528, pp. 6059–65.

    Article  CAS  Google Scholar 

Download references

Acknowledgment

Financial support from MICINN (Project MAT2009-14452) is gratefully acknowledged.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Carmen M. Cepeda-Jiménez.

Additional information

Manuscript submitted August 9, 2011.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Cepeda-Jiménez, C.M., García-Infanta, J.M., Rauch, E.F. et al. Influence of Processing Severity During Equal-Channel Angular Pressing on the Microstructure of an Al-Zn-Mg-Cu Alloy. Metall Mater Trans A 43, 4224–4236 (2012). https://doi.org/10.1007/s11661-012-1206-5

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11661-012-1206-5

Keywords

Navigation