Ultrafine Grain Formation in Ferritic Stainless Steel during Severe Plastic Deformation

Article

Abstract

The development of submicrocrystalline structures in Fe-20 pct Cr ferritic stainless steel was studied in multidirectional forging to large total strains. The structural changes are characterized by the development of microshear bands in high density dislocation substructures. The multidirectional deformation promotes the multiple shearing, which results in the formation of a spatial net of mutually crossed microshear bands subdividing the original grains. The new grains with high-angle boundaries appear primarily at the microshear band intersections and subsequently along the bands. The fraction of ultrafine grains gradually increases with increasing the density of microshear bands as a result of continuous increase in misorientations among deformation subgrains during processing. An increase in the processing temperature can accelerate remarkably the kinetics of ultrafine grain evolution at large strains. The mechanism of strain-induced grain formation is discussed in detail.

Keywords

Total Strain Dynamic Recovery Ferritic Stainless Steel Equal Channel Angular Extrusion Deformation Microstructure 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

Notes

Acknowledgments

The financial support received from the Ministry of Education, Science and Culture, Japan, under a Grant-in-Aid for Scientific Research on Priority Areas “Giant Straining Process for Advanced Materials Containing Ultra-High Density Lattice Defects” is gratefully acknowledged. Also, the authors thank Messrs. K. Usui and T. Koba for their assistance with TEM observations.

References

  1. 1.
    Y. Wang, M. Chen, F. Zhou, E. Ma: Nature, 2002, vol. 419, pp. 912–15CrossRefGoogle Scholar
  2. 2.
    V.V. Stolyarov, R.Z. Valiev, and Y.T. Zhu: Appl. Phys. Lett., 2006, vol. 88, Art. no. 041905Google Scholar
  3. 3.
    F. Musin, R. Kaibyshev, Y. Motohashi, G. Itoh: Scripta Mater., 2004, vol. 50, pp. 511–16CrossRefGoogle Scholar
  4. 4.
    H. Gleiter: Progr. Mater. Sci., 1989, vol. 33, pp. 223–315CrossRefGoogle Scholar
  5. 5.
    R.Z. Valiev, R.K. Islamgaliev, I.V. Alexandrov: Progr. Mater. Sci., 2000, vol. 45, pp. 103–89CrossRefGoogle Scholar
  6. 6.
    R.Z. Valiev, Y. Estrin, Z. Horita, T.G. Langdon, M.J. Zehetbauer, Y.T. Zhu: JOM, 2006, vol. 58, pp. 33–39CrossRefGoogle Scholar
  7. 7.
    C.C. Koh: Nanostr. Mater., 1997, vol. 9, pp. 13–22CrossRefGoogle Scholar
  8. 8.
    S. Takaki, T. Tsuchiyama, K. Nakashima, H. Hidaka, K. Kawasaki, Y. Futamura: Met. Mater. Int., 2004, vol. 10, pp. 533–39Google Scholar
  9. 9.
    I. Saunders J. Nutting: Met. Sci., 1984, vol.18, pp. 571–75Google Scholar
  10. 10.
    V.M. Segal, V.I. Reznikov, A.E. Drobyshevskiy, V.I. Kopylov: Russ. Metall., 1981, vol. 1, pp. 115–23Google Scholar
  11. 11.
    Y. Iwahashi, Z. Horita, M. Nemoto, T.G. Langdon: Acta Mater., 1997, vol. 45, pp. 4733–41CrossRefGoogle Scholar
  12. 12.
    N. Tsuji: in Severe Plastic Deformation, A. Burhanettin, ed., Nova Science, New York, NY, 2005, pp. 543–64Google Scholar
  13. 13.
    J. Wadsworth, O.D. Sherby: Progr. Mater. Sci., 1980, vol. 25, pp. 35–68CrossRefGoogle Scholar
  14. 14.
    A. Belyakov, W. Gao, H. Miura, T. Sakai: Metall. Mater. Trans. A, 1998, vol. 29A, pp. 2957–65CrossRefGoogle Scholar
  15. 15.
    A. Belyakov, K. Tsuzaki, H. Miura, T. Sakai: Acta Mater., 2003, vol. 51, pp. 847–61CrossRefGoogle Scholar
  16. 16.
    T. Sakai, H. Miura, and X. Yang: Mater. Sci. Eng. A, in pressGoogle Scholar
  17. 17.
    B. Bay, N. Hansen, D.A. Hughes, D. Kuhlmann-Wilsdorf: Acta Metall. Mater., 1992, vol. 40, pp. 205–19CrossRefGoogle Scholar
  18. 18.
    F.J. Humphreys, P.B. Prangnell, J.R. Bowen, A. Gholinia, C. Harris: Phil. Trans. R. Soc. London, 1999, vol. 357, pp. 1663–81CrossRefGoogle Scholar
  19. 19.
    P.B. Prangnell, J.R. Bowen, A. Gholinia: in Science of Metastable and Nanocrystalline Alloys, A.R. Dinesen, M. Eldrup, D. Juul Jensen, S. Linderoth, T.B. Pedersen, N.H. Pryds, S.A. Pedersen, J.A. Wert, eds., Risø National Laboratory, Roskilde, Denmark, 2001, pp. 105–26Google Scholar
  20. 20.
    A. Belyakov, T. Sakai, H. Miura, K. Tsuzaki: Phil. Mag. A, 2001, vol. 81, pp. 2629–43CrossRefGoogle Scholar
  21. 21.
    O. Sitdikov, T. Sakai, A. Goloborodko, H. Miura, R. Kaibyshev: Phil. Mag., 2005, vol. 85, pp. 1159–75CrossRefGoogle Scholar
  22. 22.
    M. Umemoto: Mater. Trans., 2003, vol. 44, pp. 1900–11CrossRefGoogle Scholar
  23. 23.
    A. Belyakov, Y. Kimura, K. Tsuzaki: Acta Mater., 2006, vol. 54, pp. 2521–32CrossRefGoogle Scholar
  24. 24.
    A. Belyakov, M. Murayama, Y. Sakai, K. Tsuzaki, M. Okubo, M. Eto, T. Kimura: J. Electron. Mater., 2006, vol. 35, pp. 2000–08CrossRefGoogle Scholar
  25. 25.
    T. Inoue, F. Yin, Y. Kimura: Mater. Sci. Eng. A, 2007, vol. A466, pp. 114–22Google Scholar
  26. 26.
    S.V.S. Narayana Murty, S. Torizuka, K. Nagai: Mater. Trans., 2005, vol. 46, pp. 2454–60CrossRefGoogle Scholar
  27. 27.
    C. Kobayashi, T. Sakai, A. Belyakov, H. Miura: Phil. Mag. Lett., 2007, vol. 87, pp. 751–66CrossRefGoogle Scholar
  28. 28.
    I. Mazurina, T. Sakai, H. Miura, O. Sitdikov, and R. Kaibyshev: Mater. Sci. Eng. A, 2008, vol. 486, pp. 662–71CrossRefGoogle Scholar
  29. 29.
    H.J. McQueen, J.J. Jonas: in Treatise on Materials Science and Technology, R.J. Arsenault, ed., Academic Press, New York, NY, 1975, pp. 393–493Google Scholar
  30. 30.
    J. Gill Sevillano, P. Van Houtte, E. Aernoudt: Progr. Mater. Sci., 1981, vol. 25, pp. 69–412CrossRefGoogle Scholar
  31. 31.
    T. Sakai, J.J. Jonas: Acta Metall., 1984, vol. 32, pp. 189–209CrossRefGoogle Scholar
  32. 32.
    T. Sakai and J.J. Jonas: in Encyclopedia of Materials: Science and Technology, K.H. Buschow, R.W. Cahn, M.C. Flemings, B. Ilschner, E.J. Kramer, and S. Mahajan, eds., Elsevier, Oxford, United Kingdom, 2001, vol. 7, pp. 7079–84Google Scholar
  33. 33.
    A. Dehghan-Manshadi, M.R. Barnett, and P.D. Hodgson: Mater. Sci. Eng. A, 2008, vol. 485, pp. 664–72CrossRefGoogle Scholar
  34. 34.
    G. Langford, M. Cohen: Metall. Trans. A, 1975, vol. 6A, pp. 901–10Google Scholar
  35. 35.
    D. Dorner, Y. Adachi, K. Tsuzaki: Scripta Mater., 2007, vol. 57, pp. 775–78CrossRefGoogle Scholar

Copyright information

© The Minerals, Metals & Materials Society and ASM International 2008

Authors and Affiliations

  1. 1.Department of Mechanical Engineering and Intelligent SystemsUEC Tokyo (The University of Electro-Communications)Chofu, TokyoJapan
  2. 2.Structural Metals CenterNational Institute for Materials ScienceTsukuba, IbarakiJapan
  3. 3.Belgorod State UniversityBelgorodRussia

Personalised recommendations