Ultrafine Grain Formation in Ferritic Stainless Steel during Severe Plastic Deformation
- 566 Downloads
- 44 Citations
Abstract
The development of submicrocrystalline structures in Fe-20 pct Cr ferritic stainless steel was studied in multidirectional forging to large total strains. The structural changes are characterized by the development of microshear bands in high density dislocation substructures. The multidirectional deformation promotes the multiple shearing, which results in the formation of a spatial net of mutually crossed microshear bands subdividing the original grains. The new grains with high-angle boundaries appear primarily at the microshear band intersections and subsequently along the bands. The fraction of ultrafine grains gradually increases with increasing the density of microshear bands as a result of continuous increase in misorientations among deformation subgrains during processing. An increase in the processing temperature can accelerate remarkably the kinetics of ultrafine grain evolution at large strains. The mechanism of strain-induced grain formation is discussed in detail.
Keywords
Total Strain Dynamic Recovery Ferritic Stainless Steel Equal Channel Angular Extrusion Deformation MicrostructureNotes
Acknowledgments
The financial support received from the Ministry of Education, Science and Culture, Japan, under a Grant-in-Aid for Scientific Research on Priority Areas “Giant Straining Process for Advanced Materials Containing Ultra-High Density Lattice Defects” is gratefully acknowledged. Also, the authors thank Messrs. K. Usui and T. Koba for their assistance with TEM observations.
References
- 1.Y. Wang, M. Chen, F. Zhou, E. Ma: Nature, 2002, vol. 419, pp. 912–15CrossRefGoogle Scholar
- 2.V.V. Stolyarov, R.Z. Valiev, and Y.T. Zhu: Appl. Phys. Lett., 2006, vol. 88, Art. no. 041905Google Scholar
- 3.F. Musin, R. Kaibyshev, Y. Motohashi, G. Itoh: Scripta Mater., 2004, vol. 50, pp. 511–16CrossRefGoogle Scholar
- 4.H. Gleiter: Progr. Mater. Sci., 1989, vol. 33, pp. 223–315CrossRefGoogle Scholar
- 5.R.Z. Valiev, R.K. Islamgaliev, I.V. Alexandrov: Progr. Mater. Sci., 2000, vol. 45, pp. 103–89CrossRefGoogle Scholar
- 6.R.Z. Valiev, Y. Estrin, Z. Horita, T.G. Langdon, M.J. Zehetbauer, Y.T. Zhu: JOM, 2006, vol. 58, pp. 33–39CrossRefGoogle Scholar
- 7.C.C. Koh: Nanostr. Mater., 1997, vol. 9, pp. 13–22CrossRefGoogle Scholar
- 8.S. Takaki, T. Tsuchiyama, K. Nakashima, H. Hidaka, K. Kawasaki, Y. Futamura: Met. Mater. Int., 2004, vol. 10, pp. 533–39Google Scholar
- 9.I. Saunders J. Nutting: Met. Sci., 1984, vol.18, pp. 571–75Google Scholar
- 10.V.M. Segal, V.I. Reznikov, A.E. Drobyshevskiy, V.I. Kopylov: Russ. Metall., 1981, vol. 1, pp. 115–23Google Scholar
- 11.Y. Iwahashi, Z. Horita, M. Nemoto, T.G. Langdon: Acta Mater., 1997, vol. 45, pp. 4733–41CrossRefGoogle Scholar
- 12.N. Tsuji: in Severe Plastic Deformation, A. Burhanettin, ed., Nova Science, New York, NY, 2005, pp. 543–64Google Scholar
- 13.J. Wadsworth, O.D. Sherby: Progr. Mater. Sci., 1980, vol. 25, pp. 35–68CrossRefGoogle Scholar
- 14.A. Belyakov, W. Gao, H. Miura, T. Sakai: Metall. Mater. Trans. A, 1998, vol. 29A, pp. 2957–65CrossRefGoogle Scholar
- 15.A. Belyakov, K. Tsuzaki, H. Miura, T. Sakai: Acta Mater., 2003, vol. 51, pp. 847–61CrossRefGoogle Scholar
- 16.T. Sakai, H. Miura, and X. Yang: Mater. Sci. Eng. A, in pressGoogle Scholar
- 17.B. Bay, N. Hansen, D.A. Hughes, D. Kuhlmann-Wilsdorf: Acta Metall. Mater., 1992, vol. 40, pp. 205–19CrossRefGoogle Scholar
- 18.F.J. Humphreys, P.B. Prangnell, J.R. Bowen, A. Gholinia, C. Harris: Phil. Trans. R. Soc. London, 1999, vol. 357, pp. 1663–81CrossRefGoogle Scholar
- 19.P.B. Prangnell, J.R. Bowen, A. Gholinia: in Science of Metastable and Nanocrystalline Alloys, A.R. Dinesen, M. Eldrup, D. Juul Jensen, S. Linderoth, T.B. Pedersen, N.H. Pryds, S.A. Pedersen, J.A. Wert, eds., Risø National Laboratory, Roskilde, Denmark, 2001, pp. 105–26Google Scholar
- 20.A. Belyakov, T. Sakai, H. Miura, K. Tsuzaki: Phil. Mag. A, 2001, vol. 81, pp. 2629–43CrossRefGoogle Scholar
- 21.O. Sitdikov, T. Sakai, A. Goloborodko, H. Miura, R. Kaibyshev: Phil. Mag., 2005, vol. 85, pp. 1159–75CrossRefGoogle Scholar
- 22.M. Umemoto: Mater. Trans., 2003, vol. 44, pp. 1900–11CrossRefGoogle Scholar
- 23.A. Belyakov, Y. Kimura, K. Tsuzaki: Acta Mater., 2006, vol. 54, pp. 2521–32CrossRefGoogle Scholar
- 24.A. Belyakov, M. Murayama, Y. Sakai, K. Tsuzaki, M. Okubo, M. Eto, T. Kimura: J. Electron. Mater., 2006, vol. 35, pp. 2000–08CrossRefGoogle Scholar
- 25.T. Inoue, F. Yin, Y. Kimura: Mater. Sci. Eng. A, 2007, vol. A466, pp. 114–22Google Scholar
- 26.S.V.S. Narayana Murty, S. Torizuka, K. Nagai: Mater. Trans., 2005, vol. 46, pp. 2454–60CrossRefGoogle Scholar
- 27.C. Kobayashi, T. Sakai, A. Belyakov, H. Miura: Phil. Mag. Lett., 2007, vol. 87, pp. 751–66CrossRefGoogle Scholar
- 28.I. Mazurina, T. Sakai, H. Miura, O. Sitdikov, and R. Kaibyshev: Mater. Sci. Eng. A, 2008, vol. 486, pp. 662–71CrossRefGoogle Scholar
- 29.H.J. McQueen, J.J. Jonas: in Treatise on Materials Science and Technology, R.J. Arsenault, ed., Academic Press, New York, NY, 1975, pp. 393–493Google Scholar
- 30.J. Gill Sevillano, P. Van Houtte, E. Aernoudt: Progr. Mater. Sci., 1981, vol. 25, pp. 69–412CrossRefGoogle Scholar
- 31.T. Sakai, J.J. Jonas: Acta Metall., 1984, vol. 32, pp. 189–209CrossRefGoogle Scholar
- 32.T. Sakai and J.J. Jonas: in Encyclopedia of Materials: Science and Technology, K.H. Buschow, R.W. Cahn, M.C. Flemings, B. Ilschner, E.J. Kramer, and S. Mahajan, eds., Elsevier, Oxford, United Kingdom, 2001, vol. 7, pp. 7079–84Google Scholar
- 33.A. Dehghan-Manshadi, M.R. Barnett, and P.D. Hodgson: Mater. Sci. Eng. A, 2008, vol. 485, pp. 664–72CrossRefGoogle Scholar
- 34.G. Langford, M. Cohen: Metall. Trans. A, 1975, vol. 6A, pp. 901–10Google Scholar
- 35.D. Dorner, Y. Adachi, K. Tsuzaki: Scripta Mater., 2007, vol. 57, pp. 775–78CrossRefGoogle Scholar