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Voltammetric detection of gliclazide and glibenclamide with graphite screen-printed electrode modified with nanopetal-structured MoWS2

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Abstract

An oversimplified and sensitive sensor based on MoWS2-modified screen-printed electrode (MoWS2/SPE) was designed in this study for detecting gliclazide (GLZ) and glibenclamide (GLB) that are two widespread employed drugs in treating noninsulin-dependent diabetes mellitus. MoWS2 exhibited very good electrocatalytic activities toward oxidation of GLZ and GLB in comparison with bare SPE in 0.1 M PBS, and the isolated capacities of oxidation peak assured concurrent determination of GLZ with widespread linear range between 0.06 and 500.0 μM. Determination limit of GLZ has been 18.0 nM (S/N  =  3). MoWS2/SPE has good steadiness, repeatability, and reproducibility. This procedure has had a successful application in detecting GLZ and GLB in their biological and pharmaceutical specimens with acceptable recovery.

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Correspondence to Somayeh Tajik or Hadi Beitollahi.

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Jahani, P.M., Tajik, S., Beitollahi, H. et al. Voltammetric detection of gliclazide and glibenclamide with graphite screen-printed electrode modified with nanopetal-structured MoWS2. Res Chem Intermed 46, 837–852 (2020) doi:10.1007/s11164-019-03993-z

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Keywords

  • Gliclazide
  • Glibenclamide
  • MoWS2 composite
  • Graphite screen-printed electrode