Research on Chemical Intermediates

, Volume 44, Issue 5, pp 3249–3265 | Cite as

MCM-41@Cu–Fe–LDH magnetic nanoparticles modified with cationic surfactant for removal of Alizarin Yellow from water samples and its determination with HPLC

  • Laleh Adlnasab
  • Maryam Ezoddin
  • Mohammad Ali Karimi
  • Najmeh Hatamikia
Article
  • 68 Downloads

Abstract

An adsorbent formed from MCM-41 and layered double hydroxides (LDH) coated on magnetic nanoparticles was synthesized and modified with a cationic surfactant (Fe3O4@MCM@Cu–Fe–LDH) for use in dispersive micro solid-phase extraction for removal of Alizarin Yellow (AY) (an anionic dye) prior to high-performance liquid chromatography–ultraviolet (HPLC–UV) detection. This adsorbent was obtained from mesopore MCM-41 coated with Fe3O4 as main core and Cu–Fe–layered double hydroxide (Cu–Fe–LDH) as nanoplatelet shell. The adsorbent was characterized by Fourier-transform infrared (FT-IR) spectroscopy, X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy-dispersive X-ray (EDX) analyses. Also, the surface morphology, Brunauer–Emmett–Teller (BET) specific surface area, and Barrett–Joyner–Halenda (BJH) pore size of the adsorbent were obtained. The adsorption isotherms were studied based on the Langmuir and Freundlich models. Adsorption data were successfully fit using the Langmuir model, showing maximum adsorption capacity of 121.95 mg g−1. The proposed method showed good linearity for AY with correlation coefficient R2 > 0.9998. The limit of detection was 0.5 µg L−1. Precision of 6.5% was obtained, as relative standard deviation (RSD) (n = 6). The method was successfully applied to determine AY in well and wastewater samples.

Keywords

Layered double hydroxides Cationic surfactant Mesopore Alizarin Yellow Langmuir and Freundlich isotherm Well and wastewater samples 

Notes

Acknowledgements

Support of this investigation by the research council of Payame Noor University is gratefully acknowledged.

Compliance with ethical standards

Conflict of interest

The authors declare that there are no conflicts of interest.

References

  1. 1.
    M.B. Gholivand, Y. Yamini, M. Dayeni, Sh Seidi, E. Tahmasebi, J. Environ. Chem. Eng. 3, 529 (2015)CrossRefGoogle Scholar
  2. 2.
    K.T. Chung, S.E. Stevens Jr, Environ. Toxicol. Chem. 12, 2121 (1993)Google Scholar
  3. 3.
    L. Calvosa, A. Monteverdi, B. Rindone, G. Riva, Water Res. 25, 985 (1991)CrossRefGoogle Scholar
  4. 4.
    Y. Wang, Y. Zhao, Y. Ma, H. Liu, T. Wei, J. Mol. Catal. A Chem. 325, 79 (2010)CrossRefGoogle Scholar
  5. 5.
    M. Abbasi, J. Clean. Prod. 145, 105 (2017)CrossRefGoogle Scholar
  6. 6.
    Y. Zhu, P. Kolar, J. Environ. Chem. Eng. 2, 2050 (2014)CrossRefGoogle Scholar
  7. 7.
    S. Wang, H. Wu, J. Hazard. Mater. 136, 482 (2006)CrossRefGoogle Scholar
  8. 8.
    Y.X. Yang, J. Ma, Q.D. Qin, X.D. Zhai, J. Mol. Catal. A Chem. 267, 41 (2007)CrossRefGoogle Scholar
  9. 9.
    Y. Huang, J. Li, X. Chen, X. Wang, RSC Adv. 4, 62160 (2014)CrossRefGoogle Scholar
  10. 10.
    S. Zhang, M. Zeng, W. Xu, J. Li, J. Xu, X. Wang, Dalton Trans. 42, 7854 (2013)CrossRefGoogle Scholar
  11. 11.
    D. Shao, G. Hou, J. Li, T. Wen, X. Ren, X. Wang, Chem. Eng. J. 255, 604 (2014)CrossRefGoogle Scholar
  12. 12.
    E. Kazemi, A.M. Haji Shabani, Sh Dadfarnia, A. Abbasi, M.R. RashidianVaziri, A. Behjat, Anal. Chim. Acta 905, 85 (2016)CrossRefGoogle Scholar
  13. 13.
    W.H. Chung, S.H. Tzing, W.H. Ding, J. Chromatogr. A 1307, 34 (2013)CrossRefGoogle Scholar
  14. 14.
    S.P. Gao, T.H. Lu, S.P. Li, H. Zhong, Colloid Surf. A 351, 26 (2009)CrossRefGoogle Scholar
  15. 15.
    F. Kovanda, E. Jindová, K. Lang, P. Kubát, Z. Sedláková, Appl. Clay Sci. 48, 260 (2010)CrossRefGoogle Scholar
  16. 16.
    A.A. Matin, P. Biparva, H. Amanzadeh, K. Farhadi, Talanta 103, 207 (2013)CrossRefGoogle Scholar
  17. 17.
    Y.L. Liu, J.B. Zhou, R.S. Zhao, X.F. Chen, Anal. Bioanal. Chem. 404, 1603 (2012)CrossRefGoogle Scholar
  18. 18.
    H. Abdolmohammad-Zadeh, K. Tavarid, Z. Talleb, Sci. World J. 2012, 1 (2012)CrossRefGoogle Scholar
  19. 19.
    H. Abdolmohammad-Zadeh, S. Kohansal, G.H. Sadeghi, Talanta 84, 368 (2011)CrossRefGoogle Scholar
  20. 20.
    H. Abdolmohammad-Zadeh, Z. Rezvani, G.H. Sadeghi, E. Zorufi, Anal. Chim. Acta 685, 212 (2011)CrossRefGoogle Scholar
  21. 21.
    M. Saraji, M. Ghani, J. Chromatogr. A 1366, 24 (2014)CrossRefGoogle Scholar
  22. 22.
    G. Giakisikli, A.N. Anthemidis, Anal. Chim. Acta 789, 1 (2013)CrossRefGoogle Scholar
  23. 23.
    M. Shao, F. Ning, J. Zhao, M. Wei, D.G. Evans, X. Duan, J. Am. Chem. Soc. 134, 1071 (2012)CrossRefGoogle Scholar
  24. 24.
    H. Zhang, G. Zhang, X. Bi, X. Chen, J. Mater. Chem. A 1, 5934 (2013)CrossRefGoogle Scholar
  25. 25.
    F. Mi, X. Chen, Y. Ma, S. Yin, F. Yuan, H. Zhang, Chem. Commun. 47, 12804 (2011)CrossRefGoogle Scholar
  26. 26.
    D. Pan, H. Zhang, T. Fan, J. Chen, X. Duan, Chem. Commun. 47, 908 (2011)CrossRefGoogle Scholar
  27. 27.
    Y. Zhao, S. He, M. Wei, D.G. Evans, X. Duan, Chem. Commun. 46, 3031 (2010)CrossRefGoogle Scholar
  28. 28.
    A. Wongariyakawee, F. Schäeffel, J.H. Warner, D. O’Hare, J. Mater. Chem. 22, 7751 (2012)CrossRefGoogle Scholar
  29. 29.
    H. Zhang, D. Pan, K. Zou, J. He, X. Duan, J. Mater. Chem. 19, 3069 (2009)CrossRefGoogle Scholar
  30. 30.
    X. Zhao, Sh Liu, P. Wang, Zh Tang, H. Niu, Y. Cai, F. Wu, H. Wang, W. Meng, J.P. Giesy, J. Chromatogr. A 1414, 22 (2015)CrossRefGoogle Scholar
  31. 31.
    H. Niu, S. Zhang, X. Zhang, Y. Cai, ACS Appl. Mater. Interfaces 2, 1157 (2010)CrossRefGoogle Scholar
  32. 32.
    X. Zhao, Y. Shi, Y. Cai, S. Mou, Environ. Sci. Technol. 42, 1201 (2008)CrossRefGoogle Scholar
  33. 33.
    Y. Zou, Y. Chen, Z. Yan, C. Chen, J. Wang, S. Yao, Analyst 138, 5904 (2013)CrossRefGoogle Scholar
  34. 34.
    L. Sun, C. Zhang, L. Chen, J. Liu, H. Jin, H. Xu, L. Ding, Anal. Chim. Acta 638, 162 (2009)CrossRefGoogle Scholar
  35. 35.
    J. Li, X. Zhao, Y. Shi, Y. Cai, S. Mou, G. Jiang, J. Chromatogr. A 1180, 24 (2008)CrossRefGoogle Scholar
  36. 36.
    X. Yang, K. Qiao, F. Liu, X. Wu, M. Yang, J. Li, H. Gao, S. Zhang, W. Zhou, R. Lu, Talanta 166, 93 (2017)CrossRefGoogle Scholar
  37. 37.
    P. Tartaj, Chem. Commun. 47, 256 (2011)CrossRefGoogle Scholar
  38. 38.
    L. Adlnasab, H. Ebrahimzadeh, A.A. Asgharinezhad, M. Nasiri Aghdam, A. Dehghani, S. Esmaeilpour, Anal. Methods 3, 616 (2013)Google Scholar
  39. 39.
    J. Li, Q. Fan, Y. Wu, X. Wang, C. Chen, Z. Tang, X. Wang, J. Mater. Chem. A 4, 1737 (2016)CrossRefGoogle Scholar
  40. 40.
    M. Ghaedi, D. Daneshfar, A. Ahmadi, M.S. Momeni, J. Ind. Eng. Chem. 21, 587 (2015)CrossRefGoogle Scholar
  41. 41.
    V. Belessi, G. Romanos, N. Boukos, D. Lambropoulou, C. Trapalis, J. Hazard. Mater. 170, 836 (2009)CrossRefGoogle Scholar
  42. 42.
    J. Zolgharnein, N. Asanjrani, M. Bagtash, G. Azimi, Spectrochim. Acta. A Mol. Biomol. Spectrosc. 126, 291 (2014)CrossRefGoogle Scholar
  43. 43.
    S. Hashemian, M. Rahimi, A.A. Kerdegari, Desalin. Water Treat. 57, 14696 (2015)CrossRefGoogle Scholar
  44. 44.
    M. Salman, M. Athar, U. Shafique, M.I. Din, R. Rehman, A. Akram, S.Z. Ali, Turk. J. Eng. Environ. Sci. 35, 209 (2011)Google Scholar

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© Springer Science+Business Media B.V., part of Springer Nature 2018

Authors and Affiliations

  • Laleh Adlnasab
    • 1
  • Maryam Ezoddin
    • 2
  • Mohammad Ali Karimi
    • 2
  • Najmeh Hatamikia
    • 2
  1. 1.Department of Chemistry and Polymer, Faculty of Chemistry and Petrochemical EngineeringStandard Research InstituteKarajIran
  2. 2.Department of ChemistryPayame Noor UniversityTehranIran

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