Skip to main content
Log in

Microstructure and Properties of the Mullite–ZrO2(Y2O3)–Si3N4-Composite Ceramics Sintered in by Different Methods

  • Published:
Refractories and Industrial Ceramics Aims and scope

The purpose of the study was to investigate densification, phase composition, microstructure and properties of mullite–ZrO2 composite ceramics with the Si3N4 additive, sintered by various methods: conventional sintering, spark-plasma sintering, and sintering in both microwave and solar furnaces. The strength properties (compressive strength and elastic modulus) of the ceramic samples sintered by the conventional method and by spark-plasma sintering were compared. Some reasons for the formation of defects in the samples after sintering in microwave and solar furnaces are indicated

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1.
Fig. 2.
Fig. 3.
Fig. 4.
Fig. 5.
Fig. 6.
Fig. 7.
Fig. 8.

Similar content being viewed by others

References

  1. M. Malki, C. M. Hoo, M. L. Mecartery, and H. Schneider, “Electrical conductivity of mullite ceramics,” J. Am. Ceram. Soc., 97, 1923 – 1930 (2014).

    Article  CAS  Google Scholar 

  2. N. Rendtorff, L. Garrido, and E. Aglietti, “Mullitezirconiazirconcomposites: Properties and thermal shock resistance,” Ceram. Int., 35(2), 779 – 786 (2008). https://doi.org/10.1016/j.ceramint.2008.02.0/.

    Article  Google Scholar 

  3. K. Das, S. K. Das, B. Mukherjee, and G. Barnerjee, “Microstructural and mechanical properties of reaction sintered mullitezirconia composites with magnesia as additive,” Interceram., No. 5, 304 – 616 (1998).

  4. D. Pereira, G. R. S. Biasibetti, R. V. Camerini, and A. S. Pereira, “Sintering of mullite by different methods,” Materials and Manufacturing Processes, 29(4), 391 – 396 (2014). https://doi.org/10.1080/10426914.2013.864400.

    Article  CAS  Google Scholar 

  5. Kuo Hsien-Nan, Chou Jyh-Horng, and Liu Tung-Kuan, “Microstructure and mechanical properties of microwave sintered ZrO2 bioceramics with TiO2 addition,” Applied Bionics and Biomechanics, Vol. 2016, Article ID 2458685, 7 p. (2016) https://doi.org/10.1155/2016/2458685.

  6. S. Bodhak, S. Bose, and A. Bandyopadhyay, “Densification study and mechanical properties of microwave-sintered mullite and mullite-zirconia composites,” J. Am. Ceram. Soc., 94(1), 32 – 41 (2011). doi: https://doi.org/10.1111/j.1551-2916.2010.04062.x.

    Article  CAS  Google Scholar 

  7. P. M. Souto, M. A. Camerucci, A. G. T. Martinez, and R. H. G. A. Kiminami, “High-temperature diametral compression strength of microwave-sintered mullite,” J. Eur. Ceram. Soc., 31, 2819 – 2826 (2011). doi:https://doi.org/10.1016/j.jeurceramsoc.2011. 07.034.

  8. N. Zhilinska, I. Zalite, J. Rodriguez, et al., “Sintering of nanodisperse powders in a solar furnace,” Eur. Powder Met. Conf. 2003 (EuroPM 2003), Valencia, 423 – 428 (2003).

  9. R. Roman, I. Canadas, J. Rodriguez, et al., “Solar sintering of alumina ceramics: microstructural development,” Solar Energy, 82, 893 – 902 (2008). doi: https://doi.org/10.1016/j.solener.2008.04.002.

    Article  CAS  Google Scholar 

  10. G. Sedmale, M. Rundans, I. Sperberga, et al., “Ceramic of the mullite–ZrO2/Y2O3–SiAlON system during spark plasma sintering,” Refract. Ind. Ceram., 57(2), 146 – 150 (2016).

Download references

The work was financed by the European Regional Development Fund within the project 1.1.1.1/16/A/077 “Mining and synthetic nano powders for obtaining porous ceramics and modification of ceramic materials” and within the project SFERA PROJECT 2017 “Mullite-zirconia refractory materials development by solar furnace sintering”.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to G. Sedmale.

Additional information

Translated from Novye Ogneupory, No. 7, pp. 49 – 54, July 2018.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Sedmale, G., Grase, L., Zalite, I. et al. Microstructure and Properties of the Mullite–ZrO2(Y2O3)–Si3N4-Composite Ceramics Sintered in by Different Methods. Refract Ind Ceram 59, 369–374 (2018). https://doi.org/10.1007/s11148-018-0238-9

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11148-018-0238-9

Keywords

Navigation