Influence of light incident angle on reflectance spectra of metals processed by color laser marking technology

  • E. I. Ageev
  • Y. M. Andreeva
  • P. N. Brunkov
  • Y. Y. Karlagina
  • G. V. Odintsova
  • D. V. Pankin
  • S. I. Pavlov
  • V. V. Romanov
  • R. M. Yatsuk
Article
Part of the following topical collections:
  1. Fundamentals of Laser Assisted Micro- & Nanotechnologies

Abstract

A comparison of oxide films formed on the stainless steel surface during laser and furnace heating is presented. Obtained samples were examined by optical and scanning electron microscopy. In order to characterize the optical properties, reflection spectra within the wavelength range 190–900 nm were measured with a spectrophotometer equipped with the integrating sphere for incidence angles from 0° to 60°. The topology of obtained oxide films was characterized by scanning probe microscopy. Due to light interference in produced films, the coloration of treated area is observed. It was found that there is no change in the characteristic appearance of reflectance spectra at different light incidence angles, but a blue-shift occurs especially for the case of laser-induced films, which results in a visible change of surface color. This effect is associated with an interference character of originating color and features of surface relief under an oxide film.

Keywords

Color laser marking Oxide films Spectrophotometry Stainless steel Fiber laser 

References

  1. Arzuov, M.I., Barchukov, A.I., Bunkin, F.V., Kirichenko, N.A., Konov, V.I., Luk’yanchuk, B.S.: Influence of interference effects in oxide films on the kinetics of laser heating of metals. Sov. J. Quantum Electron. 9, 281–284 (1979)ADSCrossRefGoogle Scholar
  2. Chourpa, I., Douziech-Eyrolles, L., Ngaboni-Okassa, L., Fouquenet, J.-F., Cohen-Jonathan, S., Soucé, M., Marchais, H., Dubois, P.: Molecular composition of iron oxide nanoparticles, precursors for magnetic drug targeting, as characterized by confocal Raman microspectroscopy. Analyst 130, 1395–1403 (2005)ADSCrossRefGoogle Scholar
  3. Duprez, D., Cavani, F.: Handbook of Advanced Methods and Processes in Oxidation Catalysis: From Laboratory to Industry. World Scientific Publishing Co. Pte. Ltd., Singapore (2014)CrossRefGoogle Scholar
  4. Jervis, T.R., Williamson, D.L., Hirvonen, J.-P., Zocco, T.G.: Characterization of the surface oxide formed by excimer laser surface processing of AISI 304 stainless steel. Mater. Lett. 9, 379–383 (1990)CrossRefGoogle Scholar
  5. Kozakov, A.T., Yares’ko, S.I.: Using auger electron spectroscopy for studying the composition of the surface of multicomponent alloys under the effect of pulsed laser irradiation. Inorg. Mater. Appl. Res. 2, 254–260 (2011)CrossRefGoogle Scholar
  6. Łekecka, K.M., Antończak, A.J., Szubzda, B., Wójcik, M.R., Stekepak, B.D., Szymczyk, P., Trzciński, M., Ozimek, M., Abramski, K.M.: Effects of laser-induced oxidation on the corrosion resistance of AISI 304 stainless steel. J. Laser Appl. 28, 032009 (2016)CrossRefGoogle Scholar
  7. Li, Z.L., Zheng, H.Y., Teh, K.M., Liu, Y.C., Lim, G.C., Seng, H.L., Yakovlev, N.L.: Analysis of oxide formation induced by UV laser coloration of stainless steel. Appl. Surf. Sci. 256, 1582–1588 (2009)ADSCrossRefGoogle Scholar
  8. Schneider, M., Langklotz, U., Michaelis, A.: Thickness determination of thin anodic titanium oxide films—a comparison between coulometry and reflectometry. Surf. Interface Anal. 43, 1471–1479 (2011)CrossRefGoogle Scholar
  9. Simka, W., Sadkowski, A., Warczak, M., Iwaniak, A., Dercz, G., Michalska, J., Maciej, A.: Characterization of passive films formed on titanium during anodic oxidation. Electrochim. Acta 56, 8962–8968 (2011)CrossRefGoogle Scholar
  10. Somervuori, M., Johansson, L.-S., Heinonen, M.H., Van Hoecke, D.H.D., Akdut, N., Hänninen, H.E.: Characterisation and corrosion of spot welds of austenitic stainless steels. Mater. Corros. 55, 421–436 (2004)CrossRefGoogle Scholar
  11. Tepluhin, G.N., Gropyanov, A.V.: Metallovedenie i termicheskaya obrabotka (Metallurgical Science and Heat Treatment). SPbGTU RP, St. Petersburg (2011)Google Scholar
  12. Thibeau, R.J., Brown, C.W., Heidersbach, R.H.: Raman spectra of possible corrosion products of iron. Appl. Spectrosc. 32, 532–535 (1978)ADSCrossRefGoogle Scholar
  13. Veiko, V., Odintsova, G., Ageev, E., Karlagina, Y., Loginov, A., Skuratova, A., Gorbunova, E.: Controlled oxide films formation by nanosecond laser pulses for color marking. Opt. Express 22, 24342–24347 (2014)ADSCrossRefGoogle Scholar
  14. Veiko, V., Odintsova, G., Gorbunova, E., Ageev, E., Shimko, A., Karlagina, Y., Andreeva, Y.: Development of complete color palette based on spectrophotometric measurements of steel oxidation results for enhancement of color laser marking technology. Mater. Des. 89, 684–688 (2016)Google Scholar
  15. Veiko, V.P., Slobodov, A.A., Odintsova, G.V.: Availability of methods of chemical thermodynamics and kinetics for the analysis of chemical transformations on metal surfaces under pulsed laser action. Laser Phys. 23, 66001 (2013)CrossRefGoogle Scholar
  16. Yun, H.-G., Kim, M., You, I.-K.: Tuned optical reflection characteristics of chemically-treated Ti substrates. ETRI J. 34, 954–957 (2012)CrossRefGoogle Scholar

Copyright information

© Springer Science+Business Media New York 2017

Authors and Affiliations

  1. 1.ITMO UniversitySt. PetersburgRussia
  2. 2.Ioffe InstituteSt. PetersburgRussia
  3. 3.St. Petersburg State UniversitySt. PetersburgRussia

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