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Journal of Nanoparticle Research

, Volume 10, Issue 8, pp 1349–1354 | Cite as

Synthesis of C–N nanotube blocks and Y-junctions in bamboo-like C–N nanotubes

  • Ram Manohar Yadav
  • Dinesh Pratap Singh
  • T. Shripathi
  • O. N. Srivastava
Brief Communication

Abstract

We report the observations made on the synthesis and characterization of C–N nanotube blocks and Y-junctions in bamboo-like C–N nanotubes. The C–N nanotube Blocks have been synthesized by pyrolyzing the mixture of silver nitrate acetonitrile solution and ferrocene benzene solution. The structural/microstructural characterization of the as-synthesized material has been done using scanning electron microscopy (SEM) and transmission electron microscopy (TEM). X-ray photoelectron spectroscopic (XPS) analysis has been carried out to confirm the presence of nitrogen in nanotubes. These investigations reveal the formation of blocks of bamboo-like nanotubes having the dimension 300 × 200 × 30 μm and the diameter is 20–50 nm. We also observe the formation of Y-junctions in bamboo-like nanotubes as we spray the acetonitrile ferrocene and AgNO3 mixture. The length of the synthesized Y-junction nanotube bundles is ~2 μm. Some more complex Ψ-shaped junctions are also found to be present. The diameters of the Y-junction nanotubes is ~80 nm at the junction and 25–50 nm at the branches.

Keywords

Nanotubes Bamboo-like Y-junction Electron microscopy Nanostructure 

Notes

Acknowledgements

The authors are extremely grateful to Prof. CNR Rao, Late Dr. A. K. Singh, Prof. R. S. Tiwari, & Prof. S. Ram for their encouragement. The authors acknowledge with gratitude the financial supports from DST:UNANST, Council of Scientific and Industrial Research (CSIR) and University Grant Commission (UGC) New Delhi, India.

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Copyright information

© Springer Science+Business Media B.V. 2008

Authors and Affiliations

  • Ram Manohar Yadav
    • 1
    • 2
  • Dinesh Pratap Singh
    • 1
  • T. Shripathi
    • 3
  • O. N. Srivastava
    • 1
  1. 1.Department of PhysicsBanaras Hindu UniversityVaranasiIndia
  2. 2.Department of PhysicsVSSD (PG) College KanpurKanpurIndia
  3. 3.UGC-DAE Consortium for Scientific ResearchIndore CentreIndoreIndia

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