Journal of Nanoparticle Research

, Volume 8, Issue 5, pp 729–736 | Cite as

Flame spray synthesis under a non-oxidizing atmosphere: Preparation of metallic bismuth nanoparticles and nanocrystalline bulk bismuth metal

Brief communication

Abstract

Metallic bismuth nanoparticles of over 98% purity were prepared by a modified flame spray synthesis method in an inert atmosphere by oxygen-deficient combustion of a bismuth-carboxylate based precursor. The samples were characterized by X-ray diffraction, thermal analysis and scanning electron microscopy confirming the formation of pure, crystalline metallic bismuth nanoparticles. Compression of the as-prepared powder resulted in highly dense, nanocrystalline pills with strong electrical conductivity and bright metallic gloss.

Keywords

bismuth metal nanoparticle flame spray reducing flame synthesis nanocrystalline metal combustion nanoengineering 

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Copyright information

© Springer Science+Business Media, Inc. 2006

Authors and Affiliations

  1. 1.Institute for Chemical and Bioengineering, ETH ZürichZurichSwitzerland

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