Selected thermoanalytical methods and their applications from medicine to construction
- 219 Downloads
- 110 Citations
Abstract
There are many thermoanalytical techniques but only several of them such as thermogravimetric analysis (TG), high resolution thermogravimetric analysis (Hi-Res™ TG), derivative thermogravimetry (DTG), differential thermal analysis (DTA), calorimetry, differential scanning calorimetry (DSC), modulated differential scanning calorimetry (MDSC), evolved gas analysis (EGA), transient thermal analysis (TTA) and thermal conductivity (k) have selected to be discussed in this paper. Simultaneous thermal analysis (STA) is ideal for investigating issues such as the glass transition of modified glasses, binder burnout, dehydration of ceramic materials or decomposition behaviour of inorganic building materials, also with gas analysis. Selected applications of various thermoanalytical techniques from medicine to construction have also been discussed in this paper.
Keywords
applications of TA DSC DTG EGA TG thermal conductivity TTAPreview
Unable to display preview. Download preview PDF.
References
- 1.M. E. Brown, Introduction to Thermal Analysis: Techniques and Applications, Kluwer Academic Publishers, 2nd Edn., (2001) p. 1–280.Google Scholar
- 2.B. Chowdhury and S. C. Mojumdar, J. Therm. Anal. Cal., 81 (2005) 179.CrossRefGoogle Scholar
- 3.B. X. Li, W. Q. Liang, W. S. Zhang and Z. He, J. Chin. Cer. Soc., 28 (2000) 325.Google Scholar
- 4.I. Janotka, CERAMICS — Silikáty, 43 (1999) 61.Google Scholar
- 5.E. W. Fischer, H. J. Sterzel and G. Wegner, Koll.-Z. Z. Polym., 251 (1973) 83.Google Scholar
- 6.S. C. Mojumdar, M. Melník and E. Jóna, J. Therm. Anal. Cal., 56 (1999) 533.CrossRefGoogle Scholar
- 7.E. Jona, E. Rudinska, M. Sapietova, M. Pajtasova and D. Ondrusova, Res. J. Chem. Environ., 10 (2006) 31.Google Scholar
- 8.D. Czakis-Sulikowska and A. Czylkowska, J. Therm. Anal. Cal., 76 (2004) 543.CrossRefGoogle Scholar
- 9.E. Dan and I. Janotka, Ceramics — Silikáty, 47 (2003) 137.Google Scholar
- 10.D. Czakis-Sulikowska and A. Czylkowska, J. Therm. Anal. Cal., 71 (2003) 395.CrossRefGoogle Scholar
- 11.R. Sun, S. T. Min and X. F. Sun, Int. J. Polym. Anal. Charact., 7 (2002) 130.CrossRefGoogle Scholar
- 12.I. Janotka and T. Nürnbergerová, Build. Res. J., 47 (1999) 143.Google Scholar
- 13.M. Day, A. V. Nawaby and X. Liao, J. Therm. Anal. Cal., 86 (2006) 623.CrossRefGoogle Scholar
- 14.D. Czakis-Sulikowska, A. Czylkowska, A. Malinowska, J. Therm. Anal. Cal., 67 (2002) 667.CrossRefGoogle Scholar
- 15.I. Janotka, Š. Kišš and R. Baslík, Appl. Clay Sci., 21 (2002) 21.CrossRefGoogle Scholar
- 16.A. Krutošíková, B. Mitasová, E. Jóna, and M. Bobošíková, Chem. Pap., 55 (2001) 290.Google Scholar
- 17.M. Drabik, S. C. Mojumdar and L. Galikova, Cem. Concr. Res., 31 (2001) 751.CrossRefGoogle Scholar
- 18.M. Pajtášová, E. Jóna and M. Koman, Challenges for Coordination Chemistry in the new Century, 5 (2001) 433.Google Scholar
- 19.S. C. Mojumdar, K. G. Varshney and A. Agrawal, Res. J. Chem. Environ., 10 (2006) 89.Google Scholar
- 20.M. Drábik, S. Balkovic, D. Tunega and V. Š. Fajnor, J. Therm. Anal. Cal., 85 (2006) 469.CrossRefGoogle Scholar
- 21.I. Janotka, L. Števula and M. D. Frt’alová, Build. Res. J., 42 (1994) 101.Google Scholar
- 22.D. Czakis-Sulikowska, A. Czylkowska and A. Malinowska, J. Therm. Anal. Cal., 65 (2001) 505.CrossRefGoogle Scholar
- 23.S. C. Mojumdar, E. Jóna and M. Melník, J. Therm. Anal. Cal., 60 (2000) 571.CrossRefGoogle Scholar
- 24.E. Jóna, A. Krutošíková and B. Mitasová, Challenges for Coordination Chemistry in the New Century, 5 (2001) 403.Google Scholar
- 25.M. Drabik, L. Galikova, Z. Sadlekova and M. Kubranova, J. Thermal Anal., 46 (1996) 479.CrossRefGoogle Scholar
- 26.S. C. Mojumdar, K. G. Varshney, P. Gupta and A. Agrawal, Res. J. Chem. Environ., 10 (2006) 85.Google Scholar
- 27.D. Czakis-Sulikowska and A. Malinowska, Pol. J. Chem., 76 (2002) 1047.Google Scholar
- 28.M. Drabik, L. Galikova, G. B. Hix, A. G. Pearce, R. C. T. Slade and K. E. Young, Cem. Concr. Res., 27 (1997) 127.CrossRefGoogle Scholar
- 29.S. C. Mojumdar, M. Melník and E. Jóna, J. Therm. Anal. Cal., 61 (2000) 915.CrossRefGoogle Scholar
- 30.S. C. Mojumdar, Res. J. Chem. Environ., 9 (2005) 23.Google Scholar
- 31.M. T. Saleh, S. C. Mojumdar and M. Lamoureux, Res. J. Chem. Environ., 10 (2006) 14.Google Scholar
- 32.Y. Masuda, Thermochim. Acta, 39 (1980) 235.CrossRefGoogle Scholar
- 33.S. C. Mojumdar, Challenges for Coord. Chemistry in the new century, 5 (2001) 453.Google Scholar
- 34.V. Zelenak, I. Cisarova, M. Sabo, P. Llewellyn and K. Gyoryova, J. Coord. Chem., 57 (2004) 87.CrossRefGoogle Scholar
- 35.S. C. Mojumdar, K. Mazanec and M. Drabik, J. Therm. Anal. Cal., 83 (2006) 135.CrossRefGoogle Scholar
- 36.V. Zelenak, M. Sabo, W. Massa and P. Llewellyn, Inorg. Chim. Acta, 357 (2004) 2049.CrossRefGoogle Scholar
- 37.V. S. Ramachandran, R. M. Paroli, J. M. Beaudoin and A. H. Delgado, Handbook of Thermal Analysis of Construction Material, Vol. 1, November 1, 2002.Google Scholar
- 38.S. C. Mojumdar, J. Therm. Anal. Cal., 64 (2001) 1133.CrossRefGoogle Scholar
- 39.S. Cakir, I. Bulut, E. Bicer, E. Coskun and O. Cakir, J. Electroanal. Chem., 511 (2001) 94.CrossRefGoogle Scholar
- 40.R. Ciach, W. Kapturkiewicz, W. Wolczyński and A. M. Zahra, J. Therm. Anal. Cal., 38 (1992) 1949.CrossRefGoogle Scholar
- 41.G. J. Lumetta, R. L. Sell and B. K. McNamara, J. Coord. Chem., 55 (2002) 651.CrossRefGoogle Scholar
- 42.P. Simon, E. Illekova and S. C. Mojumdar, J. Therm. Anal. Cal., 83 (2006) 67.CrossRefGoogle Scholar
- 43.S. Cakir, I. Bulut, E. Bicer, E. Coskun and O. Cakir, J. Coord. Chem., 56 (2003) 511.CrossRefGoogle Scholar
- 44.K. G. Varshney, V. Jain, A. Agrawal and S. C. Mojumdar, J. Therm. Anal. Cal., 86 (2006) 609.CrossRefGoogle Scholar
- 45.S. Bayari, A. Atac and S. Yurdakul, J. Mol. Struct., 655 (2003) 163.CrossRefGoogle Scholar
- 46.S. C. Mojumdar, J. Therm. Anal. Cal., 64 (2001) 629.CrossRefGoogle Scholar
- 47.A. Kundu and N. Kishore, J. Solution Chem., 32 (2003) 703.CrossRefGoogle Scholar
- 48.G. Madhurambal, P. Ramasamy, P. A. Srinivasan and S. C. Mojumdar, J. Therm. Anal. Cal., 86 (2006) 601.CrossRefGoogle Scholar
- 49.M. G. Kanatzidis and L. M. Tonge, J. Am. Chem. Soc., 109 (1987) 3797.CrossRefGoogle Scholar
- 50.K. G. Varshney, A. Agrawal and S. C. Mojumdar, J. Therm. Anal. Cal., 81 (2005) 183.CrossRefGoogle Scholar
- 51.M. Drábik, L. Gáliková, K. G. Varshney and M. A. Quraishi, J. Therm. Anal. Cal., 76 (2004) 91.CrossRefGoogle Scholar
- 52.H. Matsuyama and J. F. Young, Chem. Mater., 11 (1999) 3389.CrossRefGoogle Scholar
- 53.G. Kostrab, D. Mravec, M. Bajus, I. Janotka, Y. Sugi, S. J. Cho and J. H. Kim, Appl. Catalys. A: General, 299 (2006) 122.CrossRefGoogle Scholar
- 54.M. Drabik and R. C. T. Slade, Br. Ceram. Trans., 94 (1995) 242.Google Scholar
- 55.S. C. Mojumdar, L. Martiška, D. Valigura and M. Melník, J. Therm. Anal. Cal., 81 (2005) 243.CrossRefGoogle Scholar
- 56.L. D. Mitchell and J. Margeson, J. Therm. Anal. Cal., 86 (2006) 591.CrossRefGoogle Scholar
- 57.E. Jóna, E. Rudinská, M. Sapietová, M. Pajtášová, D. Ondrušová, V. Jorík and S. C. Mojumdar, Res. J. Chem. Environ., 9 (2005) 41.Google Scholar
- 58.Y. H. Liu, B. Ma, X. Zhao, Y. H. Deng, H. B. Zhang and Z. C. Wang, Thermochim. Acta, 433 (2005) 170.CrossRefGoogle Scholar
- 59.S. C. Mojumdar and L. Raki, J. Therm. Anal. Cal., 86 (2006) 651.CrossRefGoogle Scholar
- 60.M. Drabik, L. Galikova and S. C. Mojumdar, Key Eng. Mater., 206–213 (2002) 1867.CrossRefGoogle Scholar
- 61.M. Dovál’, M. Palou and S. C. Mojumdar, J. Therm. Anal. Cal., 86 (2006) 595.CrossRefGoogle Scholar
- 62.M. Drábik, S. C. Mojumdar and R. C. T. Slade, CERAM.-Silik., 46 (2002) 68.Google Scholar
- 63.S. C. Nayak, P. K. Das and K. K., Sahoo, Chem. Papers, 57 (2003) 91.Google Scholar
- 64.M. Drábik, L’. Gáliková, S. Balkovic and R. C. T. Slade, J. Phys. Chem. Solids, in press.Google Scholar
- 65.F. Kreith and M. S. Bohn, Principles of Heat Transfer, 5th Edition, PWS Publishing 1997, (a) Chapter 6.5.1, Page 413, (b) Table 6.3, Page 414, (c) Chapter 1.2, Page 4.Google Scholar
- 66.H. Poltz, Int. J. Heat Mass Tr., 8 (1965) 515.CrossRefGoogle Scholar
- 67.B. Stälhane and S. Pyk, Teknisk. Tidskrift, 61 (1931) 389.Google Scholar
- 68.E. F. M. van der Held, Warmte-Techniek, (1932).Google Scholar
- 69.E. F. M. van der Held and F. G. van Drunen, Physica, 15 (1949) 865.CrossRefGoogle Scholar
- 70.J. F. T. Pitman, ’Fluid Thermal Conductivity Determination by the Transient Line Source Method’, Ph.D. Thesis, University of London (1968).Google Scholar
- 71.N. Mani, Precise Determination of the Thermal Conductivity of Fluids using Absolute Transient Hot-Wire Technique, Ph.D. Thesis, University of Calgary, Canada (1971).Google Scholar
- 72.R. C. Prasad, ’Measurement of the Thermal Conductivity of Fluids’, Ph.D. Thesis, University of New Brunswick, Canada (1982).Google Scholar
- 73.J. J. DeGroot, J. Kestin and H. Sookiazian, Physica, 75 (1974) 454.CrossRefGoogle Scholar
- 74.L. Sun, ’The Simultaneous Measurement of Thermal Conductivity and Thermal Diffusivity’, Ph.D. Thesis, University of New Brunswick, Canada (2002).Google Scholar
- 75.H. C. Carslaw and J. C. Jaeger, Conduction of Heat in Solids, 2nd Ed., Oxford University Press, (London) 1959.Google Scholar
- 76.J. J. Healy, J. J. De Groot and J. Kestin, Physica, 82c (1976) 392.Google Scholar
- 77.Y. Shi, Radiation Effects in Transient Hot-Wire Technique: Simultaneous Measurement of Thermal Conductivity and Thermal Diffusivity of Propane, M.Sc.E. Thesis, University of New Brunswick, Canada (2006).Google Scholar
- 78.Y. Shi, L, Sun, J. E. S. Venart and R. C. Prasad, J. Therm. Anal. Cal., 86 (2006) 585.CrossRefGoogle Scholar
- 79.Y. Shi, L. Sun and J. E. S. Venart, J. Therm. Anal. Cal., in press.Google Scholar
- 80.S. Chew and A. Sim, 5th IPFA’ 95: Singapore, p. 181 188.Google Scholar
- 81.C. M. Badeen, Q. S. M. Kwok, Marie C. R. Vachon, R. Turcotte and D. E. G. Jones, J. Therm. Anal. Cal., 81 (2005) 225.CrossRefGoogle Scholar
- 82.S. C. Mojumdar and L. Raki, J. Therm. Anal. Cal., 82 (2005) 89.CrossRefGoogle Scholar
- 83.J. A. Dean, The Analytical Chemistry Handbook. New York. McGraw Hill, Inc. 1995. p. 15.1–15.5.Google Scholar
- 84.E. Pungor, A Practical Guide to Instrumental Analysis. Boca Raton, Florida 1995. p. 181–191.Google Scholar
- 85.S. Douglas, F. James Holler and T. Nieman, Principles of Instrumental Analysis. 5th Ed. New York 1998, p. 905.Google Scholar
- 86.S. C. Mojumdar, J. Kozankova, J. Chocholusek, J. Majling and V. Nemecek, J. Therm. Anal. Cal., 78 (2004) 73.CrossRefGoogle Scholar
- 87.M. Melník, S. C. Mojumdar and M. Koman, Pol. J. Chem., 73 (1999) 1293.Google Scholar
- 88.S. Tompa, R. E. Boswell, P. Skahan and C. Gotzmer, J. Thermal Anal., 49 (1997) 1161.CrossRefGoogle Scholar
- 89.S. C. Mojumdar, J. Kozánková, J. Chocholoušek, J. Majling and D. Fábryová, J. Therm. Anal. Cal., 78 (2004) 145.CrossRefGoogle Scholar
- 90.J. Kozánková, S. C. Mojumdar, J. Chocholoušek, J. Kákoš, M. Balog and L. Krajčová, J. Therm. Anal. Cal., 81 (2005) 191.CrossRefGoogle Scholar
- 91.I. Janotka, T. Nürnbergerová, M. Križma and L’ Bágel’, XI/LXXIII (2006) 159.Google Scholar