Synthesis and characterization of high quality {100} diamond single crystal

  • Xuejian Xie
  • Xiwei Wang
  • Yan Peng
  • Yingxin Cui
  • Xiufang Chen
  • Xiaobo Hu
  • Xiangang Xu
  • Peng Yu
  • Ruiqi Wang
Article
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Abstract

Non-destructive characterization of diamond plate can provide abundant information. Consequently, it will help improve the growth technique. In this paper, unintentionally doped {100} diamond single crystal (type Ib) was synthesized by the temperature gradient growth (TGG) method under high pressure (~6.5 GPa) and high temperature (~1500 °C) condition. The crystal morphology was observed by confocal laser scanning microscope (CLSM). The result indicated there was a pit on diamond surface. UV/Vis transmission measurement indicated the maximum transmittance of our sample was about 9% lower than that of theoretical value. Fourier-transformation infrared spectroscopy (FTIR) measurement confirmed that the nitrogen concentration was about 53 ppm. High resolution X-Ray diffractometer (HRXRD) was employed to evaluated the crystalline quality, and result showed that the full width of half maximum (FWHM) at (400) and (111) rocking curves were 56.9′′, 23.7′′, respectively, which revealed the good crystalline quality. In addition, the diffraction peak of (400) lattice plane exhibited an increase trend with the X-ray beam position, showing the (100) lattice surface was convex bended.

Keywords

Lattice Plane Synthetic Diamond Diamond Single Crystal Nitrogen Impurity Good Crystalline Quality 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.
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Notes

Acknowledgements

This work was financially supported by “Science and technology project of China State Grid Corp” under Grant SGSDDK00KJJS1600071, Natural Science Foundation of China under Grants (513230013, 61327808) and National Key Research and Development program under Grant 2016YFB0400201.

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Copyright information

© Springer Science+Business Media New York 2017

Authors and Affiliations

  • Xuejian Xie
    • 1
    • 2
  • Xiwei Wang
    • 1
    • 2
    • 3
  • Yan Peng
    • 1
    • 2
  • Yingxin Cui
    • 1
    • 2
  • Xiufang Chen
    • 1
    • 2
  • Xiaobo Hu
    • 1
    • 2
  • Xiangang Xu
    • 1
    • 2
  • Peng Yu
    • 2
    • 4
  • Ruiqi Wang
    • 2
    • 4
  1. 1.State Key Laboratory of Crystal MaterialsShandong UniversityJinanChina
  2. 2.Collaborative Innovation Center for Global Energy Interconnection (Shandong)JinanChina
  3. 3.Jinan Zhongwu New Material Co. LtdJinanChina
  4. 4.State Grid Shandong Electric Power Research InstituteJinanChina

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