Advertisement

Journal of Materials Science

, Volume 46, Issue 15, pp 5221–5226 | Cite as

Electrochemical deposition and magnetic properties of cobalt and iron thin films on substrate of KIT-6/ITO

  • Tingting Gao
  • Guangbin JiEmail author
  • Xiaofeng Chang
  • Xiaohui Lin
  • Jinsong Liu
  • M. Qamar
Article

Abstract

Cobalt and iron thin films were successfully electrodeposited on the KIT-6/ITO substrate. The films consisted of mesoporous structure (the average pore size of which was estimated at ~5 nm) and large specific surface area (431 m2/g). The nanofilms were further characterized by X-ray diffractometer, scanning electron microscope, and vibrating sample magnetometer. The results indicated that the Fe magnetic films tend to grow preferentially along Fe (002) crystal direction while the Co film grew along both (101) and (220) crystal directions. The as-obtained magnetic metal films exhibited ferromagnetic behavior and both the values of coercivities parallel to the films were examined below 50 Oe.

Keywords

BiFeO3 Mesoporous Structure Average Pore Size Magnetic Film Crystal Direction 

Notes

Acknowledgements

This study was finically supported by Natural Science Foundation of China (No. 50701024) and Natural Science Foundation of Jiangsu Province in China (No. BK2010497).

References

  1. 1.
    Mor GK, Prakasam HE, Varghese OK, Shankar K, Grimes CA (2007) Nanoletters 7:2356CrossRefGoogle Scholar
  2. 2.
    Kharisov BI, Kharissova O, Yacaman MJ (2010) Ind Eng Chem Res 49:8289CrossRefGoogle Scholar
  3. 3.
    Nielsch K, Wehrspohn RB, Barthel J, Kirschner J, Gosele U, Ficher SF, Kronmuller H (2001) Appl Phys Lett 79:1360CrossRefGoogle Scholar
  4. 4.
    Ross C, Chantrell R, Hwang M, Farhoud M, Saves T, Hao Y, Smith H, Ross F, Redidal M, Himphrey F (2000) Phys Rev B 62:14252CrossRefGoogle Scholar
  5. 5.
    McGuire TR, Potter RI (1975) IEEE Trans Magn 11:1018CrossRefGoogle Scholar
  6. 6.
    Tόth-Kadar E, Péter L, Becsei T, Tόth J, Pogány L, Tarnόczi T, Kamasa P, Bakonyi I, Láng G, Cziráki A, Schwarzacher W (2000) J Electrochem Soc 147:3311CrossRefGoogle Scholar
  7. 7.
    Hyeon T (2003) Chem Commun 927–934Google Scholar
  8. 8.
    Lafond V, Mutin PH, Vioux A (2004) Chem Mater 16:5380–5386CrossRefGoogle Scholar
  9. 9.
    Bearzotti A, Bertolo JM, Innocenzi P, Falcaro P, Traversa E (2004) J Eur Ceram Soc 24:1969CrossRefGoogle Scholar
  10. 10.
    Kim TW, Kleitz F, Paul B, Ryoo R (2005) J Am Chem Soc 127:7601CrossRefGoogle Scholar
  11. 11.
    Laha SC, Ryoo R (2003) Chem Commun 2138Google Scholar
  12. 12.
    Lv GM, Zhao R, Qian G, Qi YX, Wang XL, Suo JS (2004) J Mol Catal (China) 18:416Google Scholar
  13. 13.
    Costacurta S, Malfatti L, Innocenzi P et al (2008) Microporous Mesoporous Mater 115:338CrossRefGoogle Scholar
  14. 14.
    Jin GQ, Guo XY (2003) Microporous Mesoporous Mater 60:207CrossRefGoogle Scholar
  15. 15.
    Park JW, Park SS, Kim Y, Kim I, Chang SH (2008) ACS NANO 2:1137CrossRefGoogle Scholar
  16. 16.
    Martin CR (1994) Science 266:1961CrossRefGoogle Scholar
  17. 17.
    Hu J, Odom TW, Lieber CM (1999) Acc Chem Res 32:435CrossRefGoogle Scholar
  18. 18.
    Choi M, Heo W, Kleitz F, Ryoo R (2003) Chem Commun 1340Google Scholar
  19. 19.
    Kim H, Cho J (2008) J Mater Chem 18:771CrossRefGoogle Scholar
  20. 20.
    Oveisi H, Anand C, Mano A, Al-Deyab Sale\, Kalita P, Beitollahi A, Vinu A (2010) J Mater Chem 20:10120CrossRefGoogle Scholar
  21. 21.
    Shi YF, Guo BK, Corr SA, Shi QH, Hu YS, Heier KR, Chen L, Seshadri R, Stucky DG (2009) Nano Lett 12:4215–4220CrossRefGoogle Scholar
  22. 22.
    Brunaurr S, Emmett PH, Teller E (1938) J Am Chem Soc 60:309CrossRefGoogle Scholar
  23. 23.
    Zhang F, Yan Y, Yang H, Meng Y, Yu C, Tu B, Zhao D (2005) J Phys Chem B 109:8723CrossRefGoogle Scholar
  24. 24.
    Yoji D, Azusa T, Yasuhiro S (2010) Chem Commun (Camb) 46:6365CrossRefGoogle Scholar
  25. 25.
    Liu HR, Yan BW, Wang XZ (2008) J Cryst Growth 310:2934CrossRefGoogle Scholar

Copyright information

© Springer Science+Business Media, LLC 2011

Authors and Affiliations

  • Tingting Gao
    • 1
  • Guangbin Ji
    • 1
    Email author
  • Xiaofeng Chang
    • 1
  • Xiaohui Lin
    • 1
  • Jinsong Liu
    • 1
  • M. Qamar
    • 2
  1. 1.Department of Applied Chemistry, College of Materials Science and TechnologyNanjing University of Aeronautics and AstronauticsNanjingPeople’s Republic of China
  2. 2.Center of Excellence in Nanotechnology (CENT)King Fahd University of Petroleum and MineralsDhahranSaudi Arabia

Personalised recommendations