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Journal of Materials Science

, Volume 46, Issue 15, pp 5050–5055 | Cite as

A novel method for the synthesis of polyamide 6 magnetic microspheres

  • Yan Liu
  • Tingxiu Xie
  • Guisheng YangEmail author
Article

Abstract

Polyamide 6 (PA6) magnetic microspheres were firstly prepared via successively in situ polymerization using phase inversion technology of polymer pairs polyamide 6/polystyrene (PA6/PS) at extremely low PS content. The properties of PA6 magnetic microspheres, such as morphologies, diameter size distribution, magnetic properties, thermal stability, and the functional groups of the magnetic microspheres, were investigated by different techniques (i.e. SEM, TEM, DLS, VSM, FTIR, and DSC). The results indicated that the diameter distribution of PA6 magnetic microspheres was narrow, and the mean diameter size was about 7.7 μm. The saturation magnetization of magnetic microspheres reached 12.50 emu/g. Furthermore, the magnetic microspheres had abundant functional groups and better thermal stability.

Keywords

Differential Scanning Calorimeter Fe3O4 Particle Magnetic Microsphere Abundant Functional Group Methylene Dichloride 

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Copyright information

© Springer Science+Business Media, LLC 2011

Authors and Affiliations

  1. 1.Department of Polymer Science and EngineeringZhejiang UniversityHangzhouChina
  2. 2.Shanghai Genius Advanced Materials Co., LtdShanghaiChina

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