Journal of Materials Science

, Volume 43, Issue 16, pp 5504–5507 | Cite as

Selective synthesis of α- and β-SrHPO4 nanoparticles

  • Marcus Roming
  • Claus FeldmannEmail author


Nanoscale SrHPO4 is prepared via a polyol-mediated synthesis. The resulting particles are well crystallized, non-agglomerated, and very uniform in size and shape. By adjusting the experimental conditions, SrHPO4 can be obtained with the α-type as well as with the β-type of modification. In particular, particle diameters of 16 nm (α-SrHPO4) and 12 nm (β-SrHPO4) are obtained. The title compound is characterized by scanning electron microscopy, dynamic light scattering, X-ray powder diffraction, and infrared spectroscopy.


Dynamic Light Scattering Dynamic Light Scattering Polyol Diethylene Glycol Typical Recipe 


  1. 1.
    Fischer A, Mallat T, Baiker A (1997) Catal Today 37:167. doi: CrossRefGoogle Scholar
  2. 2.
    Louati B, Guidara K, Gargouri M, Fourati M (2005) Z Naturforsch 60a:121Google Scholar
  3. 3.
    Kim J, Noh M, Cho J, Kim HM, Kim KB (2005) J Electrochem Soc 152:A1142. doi: CrossRefGoogle Scholar
  4. 4.
    Levchik SV, Weil ED (2006) J Fire Sci 24(5):364. doi: CrossRefGoogle Scholar
  5. 5.
    Boudjada A, Masse R, Guitel JC (1978) Acta Crystallogr B 34:2692. doi: CrossRefGoogle Scholar
  6. 6.
    Taher LB, Smiri L, Laligant Y, Maisonneuve V (2000) J Solid State Chem 152:428. doi: CrossRefGoogle Scholar
  7. 7.
    Purnendu P, Ray AR, Ramanan A (2007) J Am Ceram Soc 90(4):1237. doi: CrossRefGoogle Scholar
  8. 8.
    Purnendu P, Ramanan A, Ray AR (2006) Am J Biochem. Biotechnol 2(2):61Google Scholar
  9. 9.
    Zheng Y, Cheng Y, Wang Y, Yu Y, Chen D, Bao F (2005) J Cryst Growth 280:569. doi: CrossRefGoogle Scholar
  10. 10.
    Toneguzzo P, Viau G, Acher O, Guillet F, Bruneton E, Fievet F (2000) J Mater Sci 35:3767. doi: CrossRefGoogle Scholar
  11. 11.
    Feldmann C, Jungk HO (2001) Angew Chem Int Ed 40:359. doi:10.1002/1521-3773(20010119)40:2<359::AID-ANIE359>3.0.CO;2-BCrossRefGoogle Scholar
  12. 12.
    Feldmann C, Roming M, Trampert K (2006) Small 2:1248. doi: CrossRefGoogle Scholar
  13. 13.
    LaMer VK, Dinegar RH (1950) J Am Chem Soc 72:4847. doi: CrossRefGoogle Scholar
  14. 14.
    Aia MA, Mathers JE, Mooney RW (1964) J Chem Eng Data 9:335. doi: CrossRefGoogle Scholar
  15. 15.
    Mooney RW, Aia MA, Hoffman CWW, Ropp RC (1959) J Am Chem Soc 81:827. doi: CrossRefGoogle Scholar
  16. 16.
    Ostwald W (1897) Z Phys Chem 22:289Google Scholar
  17. 17.
    Ropp RC, Aia MA, Hoffman CWW, Veleker TJ, Mooney RW (1959) Anal Chem 31:1163. doi: CrossRefGoogle Scholar
  18. 18.
    Boudjada A, Masse R, Guitel JC (1978) Acta Crystallogr B 34:2692. doi: CrossRefGoogle Scholar
  19. 19.
    Mel’nikova RY, Dzyuba ED, Pechkovskii VV, Barannikova TI, Kovalishina VI (1982) Russ J Inorg Chem 27:1724Google Scholar
  20. 20.
    Weidlein J, Müller U, Dehnicke K (1988) Schwingungsspektroskopie. Thieme Verlag, StuttgartGoogle Scholar

Copyright information

© Springer Science+Business Media, LLC 2008

Authors and Affiliations

  1. 1.Institut für Anorganische ChemieUniversität Karlsruhe (TH)KarlsruheGermany

Personalised recommendations