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Journal of Materials Science

, Volume 42, Issue 8, pp 2684–2689 | Cite as

Preparation and characterization of l-cystine and l-cysteine intercalated layered double hydroxides

  • Min Wei
  • Jian Guo
  • Zhiyu Shi
  • Qi Yuan
  • Min Pu
  • Guoying Rao
  • Xue DuanEmail author
Article

Abstract

l-cystine and l-cysteine have been intercalated into magnesium–aluminum layered double hydroxide by the methods of coprecipitation and ion-exchange. The structure and composition of the intercalated materials have been characterized by X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectroscopy and elemental analysis. For l-cysteine intercalated composites, two kinds of well-crystallized materials with different basal spacing were obtained, as a result of the different charge on an ion and orientation of the gallery anions. The schematic models of the intercalation structures were proposed. In addition, the thermal decomposition of l-cystine and l-cysteine intercalated LDHs has been investigated by means of thermogravimetry and differential thermal analysis (TG-DTA).

Keywords

Layered Double Hydroxide Basal Spacing Weight Loss Step Host Layer Monovalent Anion 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

Notes

Acknowledgments

This project was supported by the National Natural Science Foundation Major International Joint Research Program (Project No.: 20620130108), National Natural Science Foundation of China (Grant No.: 20601001), the Program for New Century Excellent Talents in University (Project No.: NCET-05-121) and the 111 Project (Project No.: B07004).

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Copyright information

© Springer Science+Business Media, LLC 2006

Authors and Affiliations

  • Min Wei
    • 1
  • Jian Guo
    • 1
  • Zhiyu Shi
    • 1
  • Qi Yuan
    • 1
  • Min Pu
    • 1
  • Guoying Rao
    • 1
  • Xue Duan
    • 1
    Email author
  1. 1.State Key Laboratory of Chemical Resource EngineeringBeijing University of Chemical TechnologyBeijing P. R. China

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