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Journal of Materials Science

, Volume 42, Issue 10, pp 3349–3352 | Cite as

Influence of the synthesis methods on the particle size of the LiVMoO6 phase

  • Margarita MilanovaEmail author
  • Reni Iordanova
  • Yanko Dimitriev
  • Krassimir Kostov
  • Sasho Vassilev
Size-Dependent Effects

Abstract

The lithiated transition metal oxide LiVMoO6 has been synthesized by a novel melt quenching method that presents some advantages as compared to the classical solid-state reaction and soft-combustion synthesis. These are: the short preparation time and the possibility to control the grain size of LiVMoO6 powders. The local structure of LiVMoO6 samples prepared in different ways was characterized by IR spectral analysis. The oxidation state of Li, V, and Mo was determined by X-ray photoelectron spectroscopy.

Keywords

MoO3 Li2O Glass Formation Region Brannerite Calculated Crystallite Size 

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Copyright information

© Springer Science+Business Media, LLC 2007

Authors and Affiliations

  • Margarita Milanova
    • 1
    Email author
  • Reni Iordanova
    • 1
  • Yanko Dimitriev
    • 2
  • Krassimir Kostov
    • 1
  • Sasho Vassilev
    • 3
  1. 1.Institute of General and Inorganic ChemistryBulgarian Academy of SciencesSofiaBulgaria
  2. 2.University of Chemical Technology and MetallurgySofiaBulgaria
  3. 3.Institute of Electrochemistry and Energy SystemsSofiaBulgaria

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