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Journal of Materials Science

, Volume 42, Issue 14, pp 5676–5679 | Cite as

Sol–gel synthesis of Ce-substituted BaFe12O19

  • Chang SunEmail author
  • Kangning Sun
Article

Abstract

Ce-substituted BaFe12O19 (BaCexFe12−xO19, x = 0, 0.01, 0.03, 0.05) was prepared by citrate sol–gel method. The thermal decomposition process of precursor was investigated by TG-DSC. The phase composition of the BaCexFe12−xO19 was characterized by X-ray powder diffraction analysis (XRD) which reveals that the BaCexFe12−xO19 crystallizes in a hexagonal structure. The lattice parameter of BaCexFe12−xO19 increases slightly when Ce was substituted into BaFe12O19. The average crystallite size calculated from the XRD line broadening is about 30–33 nm and no intermediate phases are detected in the XRD patterns. The transmission electron microscope (TEM) analysis indicates that the particles of samples obtained are the rod-like morphology.

Keywords

Microwave Absorber Hexagonal Ferrite Typical Transmission Electron Microscopy Image BaFe2O4 Ammonia Hydroxide 

Notes

Acknowledgement

This work was supported by the Natural Science Foundation of the People’s Republic of China (Grant No. 30540061, 50672051).

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Copyright information

© Springer Science+Business Media, LLC 2007

Authors and Affiliations

  1. 1.Key Laboratory of Liquid Structure and Heredity of Materials, Ministry of EducationShandong University (south part)JinanP. R. China
  2. 2.Engineering Ceramics Key Laboratory of Shandong ProvinceShandong University (south part)JinanP. R. China

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