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Hyperfine Interactions

, 239:14 | Cite as

Mossbauer spectroscopy study of Fe@ZrO2 nanocomposites formation by MA SHS technology

  • Tatiana KiselevaEmail author
  • Alexey Letsko
  • Tatiana Talako
  • Svetlana Kovaleva
  • Tatiana Grigoreva
  • Alla Novakova
  • Nikolay Lyakhov
Article
  • 57 Downloads
Part of the following topical collections:
  1. Proceedings of the International Conference on the Applications of the Mössbauer Effect (ICAME 2017), Saint-Petersburg, Russia, 3-8 September 2017

Abstract

Particles with core-in-shell structure Fe@ZrO2 were synthesized by step-by-step technology including formation of mechanically pre-activated (MA) precursors with Fe/Zr and Fe2O3/[Fe/Zr] composite structures formation following by Self-Propagated High temperature synthesis (SHS). Mossbauer spectroscopy, Transmission and Scanning electron Microscopy have been performed to study the peculiarities of local structure and its evolution through the sequential synthesis steps via various milling periods and reagent compositions. The exact conditions for iron core in oxide shell Fe@ZrO2 structure formation with promising functionality has been established.

Keywords

Mossbauer spectroscopy Nanocomposites Core-in-shell Mechanosynthesis Self propagated high temperature synthesis Iron Zirconia 

Notes

Acknowledgements

This work was supported by the Siberian Branch of the Russian Academy of Sciences, the National Academy of Science of Belarus and Moscow University Program of Development.

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Copyright information

© Springer International Publishing AG, part of Springer Nature 2018

Authors and Affiliations

  • Tatiana Kiseleva
    • 1
    Email author
  • Alexey Letsko
    • 2
  • Tatiana Talako
    • 2
  • Svetlana Kovaleva
    • 3
  • Tatiana Grigoreva
    • 4
  • Alla Novakova
    • 1
  • Nikolay Lyakhov
    • 4
  1. 1.Department of PhysicsMoscow M.V. Lomonosov State UniversityMoscowRussia
  2. 2.Institute of Powder Metallurgy NASMinskBelarus
  3. 3.United Institute of Mechanical EngineeringMinskBelarus
  4. 4.Institute of Solid State Chemistry and Mechanochemistry RASNovosibirskRussia

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