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Hyperfine Interactions

, 239:4 | Cite as

The milling effect on nickel ferrite particles studied using magnetization measurements and Mössbauer spectroscopy

  • M. V. Ushakov
  • M. I. OshtrakhEmail author
  • A. V. Chukin
  • V. Šepelák
  • I. Felner
  • V. A. Semionkin
Article
  • 93 Downloads
Part of the following topical collections:
  1. Proceedings of the International Conference on the Applications of the Mössbauer Effect (ICAME 2017), Saint-Petersburg, Russia, 3–8 September 2017

Abstract

Samples of NiFe2O4 nanoparticles N1 (nonactivated), N2 (milled for 15 min) and N3 (milled for 30 min) were studied using X-ray diffraction, scanning electron microscopy with energy dispersion spectroscopy, isothermal magnetization measurement and Mössbauer spectroscopy with respect to analyze the effect of particle milling on their magnetic properties. It was shown that an increase of the milling time lead to: (i) a decrease of particles’ size, (ii) a decrease of the saturation magnetic moment and (iii) an appearance of paramagnetic doublet in the Mössbauer spectra of NiFe2O4 nanoparticles.

Keywords

Mössbauer spectroscopy Magnetic measurements NiFe2O4 nanoparticles Milling effect Hyperfine parameters 

Notes

Acknowledgements

This work was supported by the Ministry of Education and Science of the Russian Federation (the Project # 3.1959.2017/4.6) and by the Act 211 Government of the Russian Federation, contract No. 02.A03.21.0006.

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Copyright information

© Springer International Publishing AG, part of Springer Nature 2017

Authors and Affiliations

  1. 1.Institute of Physics and TechnologyUral Federal UniversityEkaterinburgRussian Federation
  2. 2.Institute of NanotechnologyKarlsruhe Institute of TechnologyEggenstein-LeopoldshafenGermany
  3. 3.Institute of Physics, Faculty of Mining and GeologyVŠB-Technical University of OstravaOstravaCzech Republic
  4. 4.Racah Institute of PhysicsThe Hebrew UniversityJerusalemIsrael

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