Hyperfine Interactions

, 237:43 | Cite as

Synchrotron radiation based Mössbauer absorption spectroscopy of various nuclides

  • Ryo Masuda
  • Yasuhiro Kobayashi
  • Shinji Kitao
  • Masayuki Kurokuzu
  • Makina Saito
  • Yoshitaka Yoda
  • Takaya Mitsui
  • Makoto Seto
Article
Part of the following topical collections:
  1. Proceedings of the International Conference on the Applications of the Mössbauer Effect (ICAME 2015), Hamburg, Germany, 13-18 September 2015

Abstract

Synchrotron-radiation (SR) based Mössbauer absorption spectroscopy of various nuclides is reviewed. The details of the measuring system and analysis method are described. Especially, the following two advantages of the current system are described: the detection of internal conversion electrons and the close distance between the energy standard scatterer and the detector. Both of these advantages yield the enhancement of the counting rate and reduction of the measuring time. Furthermore, SR-based Mössbauer absorption spectroscopy of 40K, 151Eu, and 174Yb is introduced to show the wide applicability of this method. In addition to these three nuclides, SR-based Mössbauer absorption spectroscopy of 61Ni, 73Ge, 119Sn, 125Te, 127I, 149Sm, and 189Os has been performed. We continue to develop the method to increase available nuclides and to increase its ease of use. The complementary relation between the time-domain method using SR, such as nuclear forward scattering and the energy-domain methods such as SR-based Mössbauer absorption spectroscopy is also noted.

Keywords

Synchrotron radiation Synchrotron-radiation based Mössbauer absorption spectroscopy 40151Eu 174Yb Nuclear resonant inelastic scattering 

References

  1. 1.
    Gütlich, P., Bill, E., Trautwein, A. X.: Mössbauer spectroscopy and transition metal chemistry. Springer, Berlin (2011)CrossRefGoogle Scholar
  2. 2.
    Website of the Mössbauer Effect Data Center: http://www.medc.dicp.ac.cn/Resources.php. Accessed 29 September 2015 (2015)
  3. 3.
    Hastings, J. B., Siddons, D. P., van Bürck, U., Hollatz, R., Bergmann, U.: Mössbauer spectroscopy using synchrotron radiation. Phys. Rev. Lett. 66, 770–773 (1991)ADSCrossRefGoogle Scholar
  4. 4.
    Seto, M., Kitao, S., Kobayashi, Y., Haruki, R., Mitsui, T., Yoda, Y., Zhang, X. W., Kishimoto, S., Maeda, Y.: Nuclear resonant inelastic and forward scattering of synchrotron radiation by 40K. Hyperfine Interact 141/142, 99–108 (2002)ADSCrossRefGoogle Scholar
  5. 5.
    Bessas, D., Sergueev, I, Merkel, D. G., Chumakov, A. I., Rüffer, R., Jafari, A., Kishimoto, S., Wolny, J. A., Schünemann, V., Needham, R. J., Sadler, P. J., Herman, R. P.: Nuclear resonant scattering of synchrotron radiation by 187Os. Phys. Rev. B 91, 224102 (2015)ADSCrossRefGoogle Scholar
  6. 6.
    Sergeev, I., Chumakov, A. I., Deschaux Beaume-Dang, T. H., Rüffer, R., Strohm, C., van Bürck, U.: Nuclear forward scattering for high energy Mössbauer transitions. Phys. Rev. Lett. 99, 097601 (2007)ADSCrossRefGoogle Scholar
  7. 7.
    Bessas, D., Merkel, D. G., Chumakov, A. I., Rüffer, R., Hermann, R. P., Sergueev, I., Mahmoud, A., Klobes, B., McGuire, M. A., Sougrati, M. T., Stievano, L.: Nuclear forward scattering of synchrotron radiation by 99Ru. Phys. Rev. Lett. 113, 147–601 (2014)CrossRefGoogle Scholar
  8. 8.
    Ruby, S. L.: Mössbauer experiments without conventional sources. J. Phys. (Paris), Colloq 35, C6–209 (1974)CrossRefGoogle Scholar
  9. 9.
    Seto, M., Masuda, R., Higashitaniguchi, S., Kitao, S., Kobayashi, Y., Inaba, C., Mitsui, T., Yoda, Y.: Synchrotron-radiation-based Mössbauer spectroscopy. Phys. Rev. Lett. 102, 217–602 (2009)CrossRefGoogle Scholar
  10. 10.
    Masuda, R., Kobayashi, Y., Kitao, S., Kurokuzu, M., Saito, M., Yoda, Y., Mitsui, T., Iga, F., Seto, M.: Synchrotron radiation-based Mössbauer spectra of 174Yb measured with internal conversion electrons. Appl. Phys. Lett. 104, 082–411 (2014)CrossRefGoogle Scholar
  11. 11.
    Smirnov, G. V., Kohn, V. G.: Theory of nuclear resonant scattering of synchrotron radiation in the presence of diffusive motion of nuclei. Phys. Rev. B 52, 3356–3365 (1995)ADSCrossRefGoogle Scholar
  12. 12.
    Smirnov, G. V., van Bürck, U., Arthur, J., Brown, G. S., Chumakov, A. I., Baron, A. Q. R., Petry, W., Ruby, S. L.: Currents and fields reveal the propagation of nuclear polaritons through a resonant target. Phys. Rev. A 76, 043–811 (2007)Google Scholar
  13. 13.
    Seto, M., Masuda, R., Higashitaniguchi, S., Kitao, S., Kobayashi, Y., Inaba, C., Mitsui, T., Yoda, Y.: Mössbauer spectroscopy in the energy domain using synchrotron radiation. J. Phys. Conf. Ser. 217, 012–002 (2010)CrossRefGoogle Scholar
  14. 14.
    Nakano, T., Fukuda, N., Seto, M., Kobayashi, Y., Masuda, R., Yoda, Y., Mihara, M., Nozoe, Y.: Synchrotron-radiation-based Mössbauer spectroscopy of 40K in antiferromagnetic potassium nanoclusters in sodalite. Phys. Rev. B 91, 140101R (2015)ADSCrossRefGoogle Scholar
  15. 15.
    Kishimoto, S., Nishikido, F., Haruki, R., Shibuya, K., Koshimizu, M.: Fast scintillation detectors for high-energy X-ray region. Hyperfine Interact 204, 101–110 (2012)ADSCrossRefGoogle Scholar
  16. 16.
    Mibu, K., Seto, M., Mitsui, T., Yoda, Y., Masuda, R., Kitao, S., Kobayashi, Y., Suharyadi, E., Tanaka, M., Tsunoda, M., Yanagihara, H., Kita, E.: Studies on spintronics-related thin films using synchrotron-radiation-based Mössbauer spectroscopy. Hyperfine Interact 217, 127–135 (2013)ADSCrossRefGoogle Scholar
  17. 17.
    Kurokuzu, M., Kitao, S., Kobayashi, Y., Saito, M., Masuda, R., Mitsui, T., Yoda, Y., Seto, M.: Development of 125Te synchrotron-radiation-based Mössbauer spectroscopy. Hyperfine Interact 226, 687–691 (2014)ADSCrossRefGoogle Scholar
  18. 18.
    Yamaura, J., Ohsumi, H., Sugimoto, K., Tsutsui, S., Yoda, Y., Takeshita, S., Tokuda, A., Kitao, S., Kurokuzu, M., Seto, M., Yamauchi, I., Ohgushi, K., Takigawa, M., Arima, T., Hiroi, Z.: Phase transition magnetic structure of pyrochlore oxide Cd 2Os 2 O 7. J. Phys. Conf. Ser. 391, 012–112 (2012)CrossRefGoogle Scholar
  19. 19.
    Damjanović, L., Stucky, G. D., Srdanov, V. I.: Magnetism of F centers; indication of an antiferromagnetic phase transition in potassium-electro-sodalite. J. Serb. Chem. Soc. 65, 311–314 (2000)Google Scholar
  20. 20.
    Tou, H., Maniwa, Y., Mizoguchi, K., Damjanović, L., Srdanov, V. I.: NMR studies on antiferromagnetism in alkali-electro-sodalite. J. Magn. Magn. Mater. 226-230, 1098–1100 (2001)ADSCrossRefGoogle Scholar
  21. 21.
    Nakano, T., Suehiro, R., Hanazawa, A., Watanabe, K., Watanabe, I., Amato, A., Pratt, F. L., Nozoe, Y: μSR study on antiferromagnetism of alkali-metal clusters incorporated in zeolite sodalite. J. Phys. Soc. Jpn. 79, 073–707 (2010)Google Scholar
  22. 22.
    Nakano, T., Tsugeno, H., Hanazawa, A., Kashiwagi, T., Nozoe, Y., Hagiwara, M.: Antiferromagnetic resonance in alkali-metal clusters in sodalite. Phys. Rev. B 88, 174–401 (2013)CrossRefGoogle Scholar
  23. 23.
    Shenoy, G. K., Wagner, F. E.: Mössbauer isomer shifts. North-Holland, Amsterdam (1978)Google Scholar
  24. 24.
    Matsuoka, T., Fujihisa, H., Hirao, N., Ohishi, Y., Mitsui, T., Masuda, R., Seto, M., Yoda, Y., Shimizu, K., Machida, A., Aoki, K.: Structural and valence changes of europium hydride induced by application of high-pressure H 2. Phys. Rev. Lett. 107, 025–501 (2011)CrossRefGoogle Scholar
  25. 25.
    Hardcastle, K. I., Warf, J. C.: Rare earth-hydrogen system III. High pressure Investigations. Inorg. Chem. 5, 1728–1735 (1966)CrossRefGoogle Scholar
  26. 26.
    Henning, W., Bähre, G., Kienle, P.: Isomer shift and quadrupole splitting of the 2 +-rotational state in 174Yb. Z. Phys. 241, 138–149 (1971)ADSCrossRefGoogle Scholar
  27. 27.
    Gerdau, E., Rüffer, R., Winker, H., Tolksdorf, W., Klages, C. P., Hannon, J. P.: Nuclear bragg diffraction of synchrotron radiation in yttrium iron garnet. Phys. Rev. Lett. 54, 835–838 (1985)ADSCrossRefGoogle Scholar
  28. 28.
    Chumakov, A. I., Zelepukhin, M. V., Smirnov, G. V., van Bürck, U., Rüffer, R., Hollatz, R., Rüter, H. D., Gerdau, E.: Time spectra of a nearly-single-line pure nuclear reflection excited by synchrotron radiation. Phys. Rev. B 41, 9545–9547 (1990)ADSCrossRefGoogle Scholar
  29. 29.
    Sminov, G. V., van Bürck, U., Chumakov, A. I., Baron, A. Q. R., Rüffer, R.: Synchrotron Mössbauer source. Phys. Rev. B. 55, 5811–5815 (1997)ADSCrossRefGoogle Scholar
  30. 30.
    Leupold, O., Rupprecht, K., Wortmann, G.: Electronic and magnetic transitions in europium compounds studied by nuclear forward scattering of synchrotron radiation. Structural Chem 14, 97–107 (2003)CrossRefGoogle Scholar

Copyright information

© Springer International Publishing Switzerland 2016

Authors and Affiliations

  • Ryo Masuda
    • 1
  • Yasuhiro Kobayashi
    • 1
  • Shinji Kitao
    • 1
  • Masayuki Kurokuzu
    • 1
  • Makina Saito
    • 1
  • Yoshitaka Yoda
    • 2
  • Takaya Mitsui
    • 3
  • Makoto Seto
    • 1
    • 3
  1. 1.Research Reactor InstituteKyoto UniversitySennan-gunJapan
  2. 2.Resarch and Utilization DivisionJapan Synchrotron Radiation Research InstituteSayo-gunJapan
  3. 3.Condensed Matter Science Division, Sector of Nuclear Science ResearchJapan Atomic Energy AgencySayo-gunJapan

Personalised recommendations