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Harmonized protocol and certified reference material for the determination of extractable contents of phosphorus in freshwater sediments – A synthesis of recent works

  • V. Ruban
  • J. F. López-Sánchez
  • P. Pardo
  • G. Rauret
  • H. Muntau
  • Ph. Quevauviller
Special issue paper

Abstract

An analytical protocol for the determination of the extractable phosphorus contents in freshwater sediments has been harmonized through interlaboratory studies in the frame of the Standards Measurements and Testing Program of the European Commission. A homogeneous and stable sediment reference material has been prepared and certified on the basis of this protocol named SMT protocol, and will be available in spring of 2001. The SMT protocol, together with the reference material, are useful tools in the field of water management, especially at a time when quality assurance and data comparability are of paramount importance in laboratory analysis. The knowledge of the bioavailable forms of phosphorus is important not only for sediments but also for sludge and soils. Therefore, the SMT protocol could be extended to these materials and new CRMs could be prepared. The SMT protocol was used in a study of a reservoir, which allowed to calculate the P stock, therefore helping to predict the restoration delay of the lake. The paper describes the protocol and the CRM, and gives a brief outline of the case study.

Keywords

Phosphorus Sludge Reference Material European Commission Quality Assurance 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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Copyright information

© Springer-Verlag Berlin Heidelberg 2001

Authors and Affiliations

  • V. Ruban
    • 1
  • J. F. López-Sánchez
    • 2
  • P. Pardo
    • 2
  • G. Rauret
    • 2
  • H. Muntau
    • 3
  • Ph. Quevauviller
    • 4
  1. 1.Laboratoire Central des Ponts et Chaussées, Division Eau, BP 4129, 44341 Bouguenais cedex, France e-mail: veronique.ruban@lcpc.frFR
  2. 2.Universitat de Barcelona, Departament de Química Analítica, Marti i Franquès, 1–11, 08028 Barcelona, SpainES
  3. 3.European Commission, Environment Institute, 21020 Ispra (VA), ItalyIT
  4. 4.European Commission, DG Research (MO73 3/9), 200 rue de la Loi, 1049 Brussels, BelgiumBE

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