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Fresenius' Journal of Analytical Chemistry

, Volume 369, Issue 7–8, pp 674–679 | Cite as

Topochemical investigation of ancient manuscripts

  • B. Wagner
  • E. Bulska
  • A. Hulanicki
  • M. Heck
  • H. M. Ortner
Special issue paper

Abstract

Various modern instrumental techniques for surface analysis were applied for the non-destructive physico-chemical examination of works of art. As samples, pieces of ancient manuscripts endangered by iron-gall ink corrosion were used. Surface characterisation of the morphology of the cellulose fibres within corroded and non-corroded parts of the manuscript performed by scanning electron microscopy (SEM) showed seriously damaged cellulose fibres in the written parts. The elemental composition of selected parts of the manuscript was determined by energy dispersive X-ray fluorescence analysis (EDX). A more detailed study of the paper surface was then performed by electron probe microanalysis (EPMA). This technique yields the morphological characteristics of the surface as well as element distribution maps over the written area of the investigated manuscript.

Keywords

Scanning Electron Microscopy Elemental Composition Electron Probe Cellulose Fibre Surface Analysis 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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Copyright information

© Springer-Verlag Berlin Heidelberg 2001

Authors and Affiliations

  • B. Wagner
    • 1
  • E. Bulska
    • 1
  • A. Hulanicki
    • 1
  • M. Heck
    • 2
  • H. M. Ortner
    • 2
  1. 1.University of Warsaw, Department of Chemistry, Pasteura 1, 02 093 Warszawa, Poland e-mail: ebulska@chem.uw.edu.plPL
  2. 2.Darmstadt University of Technology, Department of Chemical Analytics, Institute of Material Science, Petersenstr. 23, 64287 Darmstadt, GermanyDE

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