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A simple and direct method for synthesis of vanadium oxide ribbon-like manobelts

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Abstract

A low-cost, a high-yielding of vanadium oxide nanobelts 2 was simply synthesized by hydrothermal treatment of our (NH4)2V3O8, 1, with deionized water at 200 °C for 3 days. The SEM observations show that ribbon-like nanobelts are about 150–300 nm wide and thousands of nanometers long. The XRD pattern reveals a set of the paper form reflections, characteristic of (001) reflections for layered phases. Based on FT-IR results and the EDX spectra, the chemical formula of the as-obtained ribbon-like could be described as VxOy.nH2O with a mixed valence V(V) and V(IV).

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Correspondence to H. Phetmung.

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Phetmung, H., Kim, T.W., Hwang, S.J. et al. A simple and direct method for synthesis of vanadium oxide ribbon-like manobelts. JICS 5, 706–711 (2008). https://doi.org/10.1007/BF03246153

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Keywords

  • Vanadium oxide ribbon-like nanobelts
  • Hydrothermal treatment
  • Mixed valences
  • Layered structure
  • A paper form