Bulletin of Materials Science

, Volume 29, Issue 1, pp 55–58 | Cite as

Synthesis and characterization of cadmium doped lead-borate glasses

  • A. A. Alemi
  • H. Sedghi
  • A. R. Mirmohseni
  • V. Golsanamlu
Ceramics and Glasses

Abstract

Cadmium doped lead-borate glasses were prepared from the melts in appropriate proportions of PbO2, H3BO3 and (15–40 mol%) CdO mixture in the temperature range 700–950°C. The infrared spectra of the glasses in the range 400–4000 cm-1 show their structures. No boroxol ring formation was observed in the structure of these glasses. Furthermore, doped cadmium atoms were not seen in tetrahedral coordination. But the conversion of three-fold to four-fold coordination of boron atoms in the structure of glasses was observed.

Keywords

Cadmium lead borate glasses 

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. Adams R V and Douglas R W 1959J. Soc. Glass Technol. 43 147Google Scholar
  2. Alemi A A and Hinatsu Y Unpublished workGoogle Scholar
  3. Biscoe J and Warren B E 1938J. Am. Ceram. Soc. 21 287CrossRefGoogle Scholar
  4. Chekhovskii V G 1985Ffisika I Khimiya Stekla 11 24 (English Translation)Google Scholar
  5. Doweidar H, Abouzeid M A and El-Damrawi G M 1991J. Phys. D: Appl. Phys. 24 2222CrossRefGoogle Scholar
  6. Galeener F L, Lucovsky G and Mikkelsen J C 1980Phys. Rev. B22 3983Google Scholar
  7. Ghoneun N A, El Batul H A, Abdel Shafi N and Azooz M H 1996Proceeding of Egyptian conference of chemistry (Egypt) p. 162Google Scholar
  8. Griscon D L 1978Borate glasses: Materials science research (New York: Plenum) Ch. 12, p.36Google Scholar
  9. Hassan A K, Torell L M, Borjesson L and Doweidar H 1992Phys. Rev. B45 12797Google Scholar
  10. Heaton H M and Moore H 1987J. Phys. Chem. Glasses 28 203Google Scholar
  11. Hinatsu Y, Doi Y, Ito K, Wakeshima M and Alemi A A 2003J. Solid State Chem. 172 438CrossRefGoogle Scholar
  12. Ito Y and Miyauchi K 1983J. Non-Cryst. Solids 57 389CrossRefGoogle Scholar
  13. Kamitsos E I and Karakassides M A 1989J. Phys. Chem. Glasses 30 19Google Scholar
  14. Kamitsos E I, Karakassides M A and Chryssikos G D 1987Phys. Chem. Glasses 91 1073CrossRefGoogle Scholar
  15. Kamitsos E I, Patsis A P, Karakassides M A and Chryssikos G D 1990J. Non-Cryst. Solids 126 52CrossRefGoogle Scholar
  16. Kanehisa M A and Elliot R J 1989Mater. Sci. Engg. B3 163CrossRefGoogle Scholar
  17. Karthikeyan B and Mohan S 2003Physica B334 298Google Scholar
  18. Kulkarni A R, Maiti H S and Paul A 1984Bull. Mater. Sci. 6 207Google Scholar
  19. Martino D Di, Santos L F, Marques A C and Almeida R M 2001J. Non-Cryst. Solids 293 394CrossRefGoogle Scholar
  20. Moe U K 1965Phys. Chem. Glasses 6 46Google Scholar
  21. Motke S G, Yawale S P and Yawale S S 2002Bull. Mater. Sci. 25 75Google Scholar
  22. Robinson J W 1991Practical handbook of spectroscopy (ed.) J W Robinson (USA: CRC Press Inc.) 1st ed., Ch. 5, p. 533Google Scholar
  23. Scholzelt H 1991Glass: nature, structure and properties (New York: Springer Verlag)Google Scholar
  24. Yawale S P, Pakade S V and Adgaonkar C S 1995Indian J. Pure & Appl. Phys. 33 35Google Scholar
  25. Yawale S S, Yawale S P and Adgaonkar C S 2000Indian J. Eng. Mater. Sci. 7 150Google Scholar
  26. Yiannopoulos Y D, Chryssikos G D and Kamitsos E I 2001Phys. Chem. Glasses 42 164Google Scholar

Copyright information

© Indian Academy of Sciences 2006

Authors and Affiliations

  • A. A. Alemi
    • 1
  • H. Sedghi
    • 1
    • 2
  • A. R. Mirmohseni
    • 1
  • V. Golsanamlu
    • 1
  1. 1.Department of Inorganic Chemistry, Faculty of ChemistryUniversity of TabrizTabrizIran
  2. 2.Department of Physics, Science FacultyUrmia UniversityIran

Personalised recommendations