Russian Chemical Bulletin

, Volume 48, Issue 3, pp 537–539 | Cite as

Macrocycle opening in crown compounds

4. Steric effects in the ring-opening reaction of the macrocycle of 4′-nitrobenzo-15-crown-5 ether under the action of amines to form podands
  • S. P. Gromov
  • S. N. Dmitrieva
Organic Chemistry

Abstract

The regioselective nucleophilic opening of the macrocycle of 4′-nitrobenzo-15-crown-5 ether under the action of amines with various structures to form nitrogen-containing podands was studied. A distinguishing characteristic feature of this reaction with aminoalcohols is the ability of the latter to form hydrogen bonds, resulting in an increase in the degree of conversion into podands.

Key words

4′-nitrobenzo-15-crown-5 ether opening of the macrocycle amines podands 

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References

  1. 1.
    S. P. Gromov, S. N. Dmitrieva, and V. E. Krasnovskii,Izv. Akad. Nauk, Ser. Khim., 1997, 540 [Russ. Chem. Bull., 1997,46, 519 (Engl. Transl.)].Google Scholar
  2. 2.
    S. P. Gromov, A. I. Vedernikov, and O. A. Fedorova,Izv. Akad. Nauk, Ser. Khim., 1995, 950 [Russ. Chem. Bull., 1995,44, 923 (Engl. Transl.)].Google Scholar
  3. 3.
    S. P. Gromov, A. I. Vedernikov, and O. A. Fedorova,Izv. Akad. Nauk, Ser. Khim., 1996, 687 [Russ. Chem. Bull., 1996,45, 648 (Engl. Transl.)].Google Scholar
  4. 4.
    R. Ungaro, B. El Haj, and J. Smid,J. Am. Chem. Soc., 1976,98, 5198.CrossRefGoogle Scholar
  5. 5.
    A. N. Kost, D. V. Yashunskii, S. P. Gromov, and R. S. Sagitullin,Khim. Geterotsikl. Soedin., 1980, 1268 [Chem. Heterocycl. Compd., 1980 (Engl. Transl.)].Google Scholar
  6. 6.
    S. P. Gromov, M. M. Bkhaumik, and Yu. G. Bundel',Khim. Geterotsikl. Soedin., 1985, 522 [Chem. Heterocycl. Compd., 1985 (Engl. Transl.)].Google Scholar

Copyright information

© Kluwer Academic/Plenum Publishers 1999

Authors and Affiliations

  • S. P. Gromov
    • 1
  • S. N. Dmitrieva
    • 1
  1. 1.Center of PhotochemistryRussian Academy of SciencesMoscowRussian Federation

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