Chromatographia

, Volume 53, Issue 5–6, pp 343–346

GC-MS identification of the flavonoid aglycones isolated from propolis

  • W. Maciejewicz
  • M. Daniewski
  • K. Bal
  • W. Markowski
Short Communications Gas Chromatography

Summary

Between six and nine flavonoids have been identified by GC-MS in five samples of propolis and in one sample of bud exudate from poplar (Populus nigra), all collected in Poland. On the basis of experimental data and data obtained by use of Drylab software, the optimum temperature programme was found for separation of reference samples of pinostrobin chalcone, pinocembrin, tectochrysin, genkwanin, chrysin, galangin, 5-hydroxy-4′,7-dimethoxyflavone, and pilloin.

Key Words

Gas chromatography-mass spectrometry Propolis Flavonoid aglycones Drylab optimization 

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Copyright information

© Friedr. Vieweg & Sohn Verlagsgesellschaft mbH 2001

Authors and Affiliations

  • W. Maciejewicz
    • 1
  • M. Daniewski
    • 2
  • K. Bal
    • 2
  • W. Markowski
    • 1
  1. 1.Department of Inorganic and Analytical ChemistryMedical UniversityLublinPoland
  2. 2.National Institute of Food and NutritionWarsawPoland

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