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Chromatographia

, Volume 32, Issue 1–2, pp 40–44 | Cite as

Analytical supercritical fluid extraction of Chinese herbal medicines

  • X. Ma
  • X. Yu
  • Z. Zheng
  • J. Mao
Originals

Summary

An analytical supercritical fluid extraction (SFE) technique, followed by GC/MS, was developed to separate and determine the volatile components in Chinese herbal medicine. Three kinds of herbs, frankincense, myrrh, andEvodia rutaecarpa were extracted and analyzed. The extraction was carried out using supercritical fluid CO2 at 20 MPa and 50°C. The main factors affecting the efficiency and selectivity of the extraction are discussed. The results revealed the potential of supercritical fluid extraction as an analytical procedure for the study of medicinal plants.

Key Words

Gas chromatography/mass spectrometry Supercritical fluid extraction Frankincense and Myrrh Evodia rutaccarpa 

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References

  1. [1]
    J. W. King, J. Chromatogr. Sci.27, 355 (1989).Google Scholar
  2. [2]
    R. W. Vannoort, J.-P. Chervet, H. Lingeman, G. J. Dejong, U. A. Th. Brinkman, J. Chromatogr.505, 45 (1990).Google Scholar
  3. [3]
    M. M. Schantz, S. N. Chesler, J. Chromatogr.363, 397 (1986).Google Scholar
  4. [4]
    S. B. Hawthorne, D. J. Miller, Anal. Chem.59, 1705 (1987).Google Scholar
  5. [5]
    S. B. Hawthorne, D. J. Miller, J. Chromatogr. Sci.24, 258 (1986).Google Scholar
  6. [6]
    N. Alexandrou, J. Pawliszyn, Anal. Chem.61, 2770 (1989).Google Scholar
  7. [7]
    E. I. Onuska, K. A. Terry, J. High Resolut. Chromatogr.12, 357 (1989).Google Scholar
  8. [8]
    V. Janda, G. Steenbeke, P. Sandra, J. Chromatogr.479, 200 (1989).Google Scholar
  9. [9]
    K. Sugiyama, M. Saito, J. Chromatogr.442, 121 (1988).Google Scholar
  10. [10]
    R. P. Adams, “Identification of Essential Oil by Ion Trap Mass Spectrometry”, Academic Press, San Diego, CA, 1989.Google Scholar
  11. [11]
    N. W. Davies, J. Chromatogr503, 1 (1990).Google Scholar
  12. [12]
    C. H. Brieskorn, P. Noble, Planta Medica44, 87 (1982).Google Scholar
  13. [13]
    S. Corsano, R. Nicoletti, Tetrahedron23, 1977 (1967).Google Scholar
  14. [14]
    R. Nicoletti, M. L. Forcellese, Tetrahedron24, 6519 (1968).Google Scholar
  15. [15]
    S. M. Abdel Wahab, E. A. Aboutabl, S. M. El-Zalabani, H. A. Fouad, H. L. De Pooter, B. El-Fallaha, Planta Medica53, 382 (1987).Google Scholar

Copyright information

© Friedr. Vieweg & Sohn Verlagsgesellschaft mbH 1991

Authors and Affiliations

  • X. Ma
    • 1
  • X. Yu
    • 1
  • Z. Zheng
    • 1
  • J. Mao
    • 1
  1. 1.Department of Applied ChemistryBeijing Institute of Chemical TechnologyBeijingChina

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