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Glass capillary gas chromatography of C1−C4 mononitroalkanes. Pre-calculation of the relative retention

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Summary

The separation of C1−C4 mononitroalkanes on four wall-coated glass open tubular (capillary) columns (liquid phases: OV-101, Ucon-LB-550X, NPGS and Carbowax 20M) was investigated. Retention indices were determined and the influence of the different factors (analysis temperature, method of determining the gas holdup time and the nature of the stationary phases) on their reproducibility were studied. Linear regression equations permit the pre-calculation of the retention indices of C1−C4 mononitroalkanes from their properties on all liquid phases studied.

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References

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    S. Boneva, I. Mladenov, P. Toromanova, N. Dimov, Chromatographia11, 26 (1978).

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    S. Boneva, N. Dimov, Zh. Anal. Khim.36, 1170 (1979).

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    N. Dimov, S. Boneva, “Oil and Chemistry” — Proceedings The Heavy-Chemical Technological Institute, Burgas (Bulgaris)2, 177 (1980).

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Dimov, N., Boneva, S. Glass capillary gas chromatography of C1−C4 mononitroalkanes. Pre-calculation of the relative retention. Chromatographia 15, 514–516 (1982). https://doi.org/10.1007/BF02260286

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Key Words

  • Glass capillary GC
  • Separation
  • Mononitroalkanes
  • Retention index
  • Pre-calculation