An attempt to prepare directly the title uranate by precipitation from uranyl solutions was successful if the preparation temperature was close to 100°C. The product was chemically and thermally analyzed, its IR spectra and X-ray patterns were taken; these results are commented and a reason for explanation of the molecular water behaviour is proposed.
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Baran, V., Šourková, L. & Spalová, J. Water-free precipitation uranate with maximum sodium content, Na/U=1.0. Journal of Radioanalytical and Nuclear Chemistry Letters 95, 331–338 (1985). https://doi.org/10.1007/BF02168030
- Physical Chemistry
- Inorganic Chemistry