Esters of cyclohexen-2-yl-1-phosphinlc acid were synthesized by the action of sodium dialkylphosphite on 3-bromocyclohexene-1.
The corresponding oxides were obtained by oxidation with acetyl hydroperoxide.
The esters of 2,3-dihydroxycyclohexylphosphinic acid were obtained by hydration of the oxide.
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B. A. Arbuzov and E. N. Dianova, Izv. AN SSSR, Otd. khim. n. 1960,1399.
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Arbuzov, B.A., Dianova, E.N. Esters of cyclohexen-2-yl-1-phosphinic acid and some of their derivatives. Russ Chem Bull 10, 1197–1200 (1961). https://doi.org/10.1007/BF01118753