Journal of Materials Science

, Volume 23, Issue 6, pp 2021–2028 | Cite as

Structure studies of non-crystalline materials by electron diffraction

  • A. Munoz
  • F. L. Cumbrera
  • R. Marquez
Article

Abstract

The ability of electron diffraction to determine the structure of non-crystalline materials has been critically revised on the basis of the main sources of error: the premature temination of the experimental intensity curve and the problems associated with the elimination of the inelastically scattered intensity. A method of studying the problem is presented and the efficacy of the most representative procedures for reducing errors in the final correlation functions is checked.

Keywords

Polymer Correlation Function Electron Diffraction Structure Study Intensity Curve 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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References

  1. 1.
    G. S. Cargill,Solid State Phys. 30 (1975) 251.Google Scholar
  2. 2.
    S. Fujime,Jpn J. Appl. Phys. 5 (1966) 778.Google Scholar
  3. 3.
    ,6 (1967) 270.Google Scholar
  4. 4.
    J. F. Graczyc andS. C. Moss,Rev. Sci. Instrum. 40 (1969) 424.Google Scholar
  5. 5.
    Y. F. Komnik,Sov. Phys. Cryst. 11 (1966) 205.Google Scholar
  6. 6.
    A. Andrievskii, I. Nabitovich andY. Voloshchuk,7 (1962) 279.Google Scholar
  7. 7.
    I. Nabitovich, Y. Stetsiv andY. Voloshchuk,12 (1968) 513.Google Scholar
  8. 8.
    J. Cornet andD. Rossier,J. Non. Cryst. Solids. 12 (1973) 85.Google Scholar
  9. 9.
    M. Gandais, M. L. Theye, S. Fisson andJ. Boissonade,Phys. Status Solidi (b) 58 (1973) 601.Google Scholar
  10. 10.
    H. Leitz andW. Buckel,Z. Phys. B 35 (1979) 73.Google Scholar
  11. 11.
    A. C. Wright andA. J. Leadbetter,Phys. Chem. Glass. 17 (1976) 122.Google Scholar
  12. 12.
    M. B. Myers andJ. Berkes,J. Non-Cryst. Solids 8–10 (1972) 804.Google Scholar
  13. 13.
    P. H. Gaskell,J. Phys. C. 12 (1979) 4337.Google Scholar
  14. 14.
    G. V. Bunton,J. Non-Cryst. Solids 6 (1971) 72.Google Scholar
  15. 15.
    J. F. Graczyk andP. Chaudharl Phys. Status Solidi (b) 58 (1973) 163.Google Scholar
  16. 16.
    H. Raith,Acta Crystallogr. A,24 (1968) 85.Google Scholar
  17. 17.
    B. J. Thijsse,J. Appl. Cryst. 17 (1984) 61.Google Scholar
  18. 18.
    R. Kaplow, S. L. Strong andB. L. Averbach,Phys. Rev. A 138 (1965) 1336.Google Scholar
  19. 19.
    P. D'Antonio, C. George andJ. Karle,J. Chem. Phys. 55 (1971) 1071.Google Scholar
  20. 20.
    C. Janot, “Les Amorpes Métalliques, Ecole d'Hiver d'Aussois” (Editions de Physique, Paris, 1983) p. 81.Google Scholar
  21. 21.
    A. Muñoz, F. L. Cumbrera andnR. Marquez, II Simposio Ibérico de Fisica dela Materia Condensada, Sevilla, 1986. (Edited by Marquez, Conde and Sousa).Google Scholar
  22. 22.
    D. B. Dove andP. N. Denbigh,Rev. Sci. Instrum. 37 (1966) 1687.Google Scholar
  23. 23.
    C. W. B. Grigson,36 (1965) 1587.Google Scholar
  24. 24.
    M. D. Rechtin andB. L. Averbach,J. Non-Cryst. Solids 12 (1973) 391.Google Scholar
  25. 25.
    Y. Waseda, “The structure of non-crystalline materials” (McGraw-Hill, New York, 1980) p. 266.Google Scholar
  26. 26.
    L. N. G. Filon,Proc. Roy. Soc. (Edinburgh) 49 (1929) 38.Google Scholar
  27. 27.
    G. S. Cargill,J. Appl. Crystallogr. 4 (1971) 277.Google Scholar
  28. 28.
    Y. Waseda,Prog. Mater. Sci. 26 (1981) 1.Google Scholar
  29. 29.
    R. A. Young andD. B. Wiles,J. Appl. Crystallogr. 15 (1982) 430.Google Scholar
  30. 30.
    L. Esquivias andF. Sanz,J. Non-Cryst. Solids 70 (1985) 221.Google Scholar
  31. 31.
    A. Rahman,J. Chem. Phys. 42 (1965) 3540.Google Scholar
  32. 32.
    P. Ascarelli,Phys. Rev. 143 (1966) 143.Google Scholar
  33. 33.
    Y. I. Stetsiv,Sov. Phys. Cryst. 18 (1973) 306.Google Scholar
  34. 34.
    J. Karle andI. L. Karle,J. Chem. Phys. 18 (1950) 957.Google Scholar
  35. 35.
    J. Dixmier, Thesis, Orsay (1986).Google Scholar
  36. 36.
    R. Narayan andS. J. Ramaseshan,J. Appl. Crystallogr 12 (1979) 585.Google Scholar
  37. 37.
    N. J. Shevchik, PhD Thesis, Harvard (1972).Google Scholar
  38. 38.
    A. Anjou andF. Sanz,J. Non-Cryst. Solids 28 (1978) 319.Google Scholar
  39. 39.
    B. E. Warren andR. L. Mozzi,J. Appl. Crystallogr. 8 (1975) 674.Google Scholar
  40. 40.
    S. S. Nandra andP. J. Grundy,J. Phys. F 7 (1977) 207.Google Scholar
  41. 41.
    J. Weis, D. Barancok andI. Cerven,Phys. Status Solidi (a) 71 (1983) K117.Google Scholar
  42. 42.
    C. Lanczos, “Discourse on Fourier Series” (Oliver and Boyd, Edinburgh, 1966) p. 61.Google Scholar
  43. 43.
    O. I. Vasin, G. I. Gladysheva andE. E. Dagman,Sov. Phys. Cryst. 28 (1983) 262.Google Scholar
  44. 44.
    A. Muñoz, F. L. Cumbrera andR. Marquez,Mater. Lett. 4 (1986) 490.Google Scholar
  45. 45.
    S. Ergun,J. Appl. Crystallogr 1 (1968) 19.Google Scholar
  46. 46.
    W. C. Sadder,J. Appl. Phys. 37 (1966) 1495.Google Scholar
  47. 47.
    A. R. Stokes,Proc. Phys. Soc. (London) 61 (1948) 382.Google Scholar
  48. 48.
    W. Ruland,J. Appl. Crystallogr. 4 (1971) 328.Google Scholar
  49. 49.
    Z. Mencik,7 (1974) 44.Google Scholar
  50. 50.
    W. Wei,J. Non-Cryst. Solids 81 (1986) 239.Google Scholar
  51. 51.
    J. More, B. Garbow andK. Hillstrom, User Guide for Minpack-1, Argonne National Laboratory Report ANL-80-74, Argonne, Illinois, 1980.Google Scholar
  52. 52.
    R. Lovell, G. R. Mitchel andA. H. Windle,Acta Crystallogr. A 35 (1979) 598.Google Scholar
  53. 53.
    R. Andonov,J. Non-Cryst. Solids 47 (1982) 297.Google Scholar

Copyright information

© Chapman and Hall Ltd. 1988

Authors and Affiliations

  • A. Munoz
    • 1
  • F. L. Cumbrera
    • 1
  • R. Marquez
    • 1
  1. 1.Departamento de OpticaFacultad de FisicaSevillaSpain

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