A spin trap study of the one-step oxidative lactonization of alkanoic acids

  • V. E. Zabarev
  • É. I. Toryanskii
  • G. I. Nikishin
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Conclusions

ESR spectroscopy and the spin trap method were used to show the intermediate formation of acyloxyl and 3-carboxyalkyl radicals in the direct oxidation of alkanoic acids to γ- lactones by the action of sodium peroxydisulfate.

Keywords

Oxidation Sodium Spectroscopy Lactone Intermediate Formation 
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Literature cited

  1. 1.
    E. I. Troyanskii, I. V. Svitan'ko, and G. I. Nikishin, Izv. Akad. Nauk SSSR, Ser. Khim., 2318 (1982).Google Scholar
  2. 2.
    G. I. Nikishin, I. V. Svitan'ko (Svitanko) and E. I. Troyanskii (E. I. Troyansky), J. Chem. Soc., Perkin Trans. 2, 595 (1983).Google Scholar
  3. 3.
    E. I. Troyanskii, I. V. Svitan'ko, and G. I. Nikishin, Izv. Akad. Nauk SSSR, Ser. Khim., 133 (1985).Google Scholar
  4. 4.
    V. E. Zubarev, The Spin Trap Method [in Russian], Izd. Mosk. Cos. Univ., Moscow (1984).Google Scholar
  5. 5.
    P. Schmid and K. U. Ingold, J. Am. Chem. Soc.,100, 2493 (1978).Google Scholar
  6. 6.
    E. K. Starostin, S. I. Moryasheva, and G. I. Nikishin, Izv. Akad. Nauk SSSR, Ser. Khim., 2048 (1974).Google Scholar
  7. 7.
    M. J. Davies, B. C. Gilbert, C. B. Thomas, and J. Young, J. Chem. Soc., Perkin Trans. 2, 1199 (1985).Google Scholar

Copyright information

© Plenum Publishing Corporation 1987

Authors and Affiliations

  • V. E. Zabarev
    • 1
    • 2
  • É. I. Toryanskii
    • 1
    • 2
  • G. I. Nikishin
    • 1
    • 2
  1. 1.N. D. Zelinskii Institute of Organic ChemistryAcademy of Sciences of the USSRMoscow
  2. 2.M. V. Lomonosov Moscow State UniversityUSSR

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