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Synthesis of N1-methyldesthiobiotin

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Conclusions

N1-Methyldesthiobiotin was synthesized by starting with the ethyl ester ofα-ketodehydrodesthiobiotin.

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Literature cited

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    M. C. Scrutton, D. B. Keech, and M. T. Utter, J. Biol. Chem.,240, 574 (1965).

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    S. I. Zav'yalov, M. P. Unanyan, G. V. Kondrat'eva, and V. V. Filippov, Izv. Akad. Nauk SSSR, Ser. Khim.,1967, 1792.

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    R. Dushinsky and L. A. Dolan, J. Am. Chem. Soc.,67, 2073 (1945).

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Author information

Additional information

We express our gratitude to prof. V. V. Filippov for testing (III) for biotin activity.

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 6, pp. 1416–1418, June, 1973.

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Zav'yalov, S.I., Zheleznaya, L.L. & Pavlova, A.B. Synthesis of N1-methyldesthiobiotin. Russ Chem Bull 22, 1380–1382 (1973). https://doi.org/10.1007/BF00928643

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Keywords

  • Ester
  • Ethyl
  • Ethyl Ester