The condensation of diethyl N-alkyl-N-hydroxymethylphosphoramidates (alkyl groups — ethyl, propyl, butyl) with methyl alcohol and with propyl, isopropyl, and butyl mercaptans has given the corresponding N-alkyl-N-methoxymethyl and N-alkyl-N-alkylthiomethyl derivatives of diethyl phosphoramidate, and these compounds have been characterized.
The reaction of acetyl chloride with the N-ethyl and N-butyl derivatives of diethyl N-hydroxymethylphosphoramidate has given the corresponding N-alkyl-N-acetoxymethylphosphoramidates.
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P. I. Alimov and O. N. Fedorova, Izd. AN SSSR, Ser. khim.,1966, 1461.
Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 6, pp. 1348–1350, June, 1967.
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Fedorova, O.N., Alimov, P.I. Some reactions of diethylN-alkyl-N-Hydroxymethylphosphoramidates. Russ Chem Bull 16, 1296–1297 (1967). https://doi.org/10.1007/BF00908294