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2-Alkylthiopropionaldehyde mercaptals

Communication 2. Elimination of thiols by acids

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Conclusions

Some 1,2-bis(alkylthio)propenes were obtained by the cleavage of thiols from the mercaptals of a 2-alkylthiopropionaldehyde in the presence of either acids or dialkyl phosphites.

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Literature cited

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    A. S. Atavin, A. I. Mikhaleva, B. A. Trofimov, G. A. Kalabin, and N. P. Vasil'ev, Izv. Akad. Nauk SSSR, Ser. Khim., 614 (1971).

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    H. C. Volger and J. F. Arens, Rec. Trav. Chim.,76, 848 (1957).

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    L. C. Rinzema, J. Stoffelsma, and J. F. Arens, Rec. Trav. Chim.,78, 354 (1959).

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    H. J. Boonstra, L. Brandsma, A. M. Wiegman, and J. F. Arens, Rec. Trav. Chim.,78, 252 (1959).

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    J. F. Arens, in: Organic Sulfur Compounds, N. Kharasch (editor), Vol. 1, Pergamon Press, Oxford-London-New York-Paris (1961), p. 257.

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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 9, pp. 2014–2016, September, 1972.

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Atavin, A.S., Trofimov, B.A., Mikhaleva, A.I. et al. 2-Alkylthiopropionaldehyde mercaptals. Russ Chem Bull 21, 1955–1956 (1972). https://doi.org/10.1007/BF00854614

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Keywords

  • Propene
  • Thiol
  • Phosphite
  • Dialkyl Phosphite