Preparation of trans 1,4-butenediol from 1,3-butadiene

  • N. G. V'yunova
Brief Communications
Received:

Summary

  1. 1.

    Trans 1,4-butenediol was prepared in good yield from 1,3-butadiene by the use of the method of Thiele and Valette.

     
  2. 2.

    Use of lower temperatures (−30 to −35°) in the bromination permits preparation of a purer 1,4-dibromide.

     
  3. 3.

    Conditions for an efficient synthesis are described.

     

Keywords

Good Yield Efficient Synthesis Valette 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.
This is a preview of subscription content, log in to check access.

Literature cited

  1. 1.
    J. Thiele, Liebigs Ann. Chem.,307, 333 (1890).Google Scholar
  2. 2.
    A. Valette, Analyt. chim. acta,13, 671 (1948).Google Scholar

Copyright information

© Consultants Bureau Enterprises Inc. 1965

Authors and Affiliations

  • N. G. V'yunova
    • 1
  1. 1.N. D. Zelinskii Institute of Organic ChemistryAcademy of SciencesUSSR

Personalised recommendations