Russian Chemical Bulletin

, Volume 44, Issue 5, pp 901–906 | Cite as

Reaction of 1-aryl-2-alkenyldiazene 1-oxides with hydrogen chloride. Novel approach to the synthesis of functionally substituted arylhydrazones

  • A. Yu. Tyurin
  • A. M. Churakov
  • E. L. Goncharova
  • S. L. Ioffe
  • Yu. A. Strelenko
  • V. A. Tartakovsky
Organic Chemistry

Abstract

The reaction of 1-aryl-2-alkenyldiazene 1-oxides with HCl yields arylhydrazones of α-chloroacyl chlorides, which eliminate HCl to give 1-aryl-2-(1-chloroalken-1-yl)diazenes. The latter add amines, alcohols, and carboxylic acids to give arylhydrazone chlorides with α-functional groups.

Key words

chlorohydrazones diazene oxides azoxyalkanes azoolefins 

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Copyright information

© Plenum Publishing Corporation 1995

Authors and Affiliations

  • A. Yu. Tyurin
    • 1
  • A. M. Churakov
    • 1
  • E. L. Goncharova
    • 1
  • S. L. Ioffe
    • 1
  • Yu. A. Strelenko
    • 1
  • V. A. Tartakovsky
    • 1
  1. 1.N. D. Zelinsky Institute of Organic ChemistryRussian Academy of SciencesMoscowRussian Federation

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