Fresenius' Zeitschrift für analytische Chemie

, Volume 328, Issue 8, pp 657–661 | Cite as

Simultanbestimmung von Si, Mn, P, Cu, Al, Ni, Cr, Mo, V, Ti, Co und As in Stählen mit ICP-AES

  • Niklaus Kläntschi
  • Arnold Esenwein
  • Thomas Müller
Originalarbeiten Fließinjektions-potentiometrie
Received:

Simultaneous determination of Si, Mn, P, Cu, Al, Ni, Cr, Mo, V, Ti, Co and As in steels by ICP-AES

Summary

A universal method for quantitative analysis of twelve elements in low-alloy steels is described. The samples are digested in a mixture of sulfuric-/nitric acid/ammonium peroxodisulfate. Si, Mn, P, Cu, Al, Ni, Cr, Mo, V, Ti, Co, As are determined in solution by ICP-AES. The procedure was tested with NBS and BCS reference samples. The analytical results are in good agreement with the certified values. With slight modifications, the method is applicable to the analysis of high-alloy steel samples.

This is a preview of subscription content, log in to check access.

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

Literatur

  1. 1.
    Burman JO (1980) In: Developments in atomic plasma spectrochemical analysis. Proc Int Winter Conference, p 564Google Scholar
  2. 2.
    Wittmann A, Hancart J, Hughes W, Ohls K (1980) In: Developments in atomic plasma spectrochemical analysis. Proc Int Winter Conference, p 550Google Scholar
  3. 3.
    Belliveau J, Griffin H, Savolainen A (1981) In: ASTM STP 747, p 77Google Scholar
  4. 4.
    Bosch H, Lohau K (1981) In: 13. Spektrometertagung. Walter de Gruyter, Berlin New York, p 189Google Scholar
  5. 5.
    Wagner A, Petin J, Majerus J (1981) In: 13. Spektrometertagung. Walter de Gruyter, Berlin New York, p 167Google Scholar
  6. 6.
    Thierig D (1982) Fresenius Z Anal Chem 310:154–159Google Scholar
  7. 7.
    Fernando LA, Heavner WD, Gabrielli CC (1986) Anal Chem 58:511–512Google Scholar
  8. 8.
    Ohls K, Koch KH (1987) Fresenius Z Anal Chem 326:520–523Google Scholar
  9. 9.
    Ohls K, Loepp H (1985) Fresenius Z Anal Chem 322:371–378Google Scholar
  10. 10.
    Kläntschi N (1980) Mater Techn 8:14–23Google Scholar
  11. 11.
    Thompson M, Walsh JN (1983) A handbook of inductively coupled plasma spectrometry. Blackie, Glasgow LondonGoogle Scholar
  12. 12.
    Koch KH, Kretschmer M, Grunenberg D (1983) Arch Eisenhüttenwes 54:359–397Google Scholar
  13. 13.
    Ohls K, Sommer D, Harrmann J, Janssen A (1981) Labor Praxis 5:1046–1052Google Scholar

Copyright information

© Springer-Verlag 1987

Authors and Affiliations

  • Niklaus Kläntschi
    • 1
  • Arnold Esenwein
    • 1
  • Thomas Müller
    • 1
  1. 1.Eidgenössische Materialprüfungs- und Versuchsanstalt, EMPADübendorfSchweiz

Personalised recommendations