Isolation and identification of decahydrotetramethylcyclopropazulenol in the essential oil of Murraya koenigii (L.) Sprengor

  • I. Waßmuth-Wagner
  • H.-O. Kalinowski
  • H. Jork
Original Papers Food Analysis

Summary

The essential oil of curry leaves contains numerous terpene and sesquiterpene hydrocarbons as well as polar compounds from which decahydrotetramethylcyclopropazulenol, selin-11-en-4α-ol and caryophyllene expoxide have been isolated and identified for the first time. This has been done with the aid both of known classical methods and of modern NMR spectroscopic techniques, such as homo- and heteronuclear COSY, COSY spectra for long-range coupling and inverse TOCSY spectra. The results are summarized and discussed.

Keywords

Physical Chemistry Analytical Chemistry Inorganic Chemistry Hydrocarbon Classical Method 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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References

  1. 1.
    Kiritikar KR, Basu BD (1959) Indian Medicinal Plants, vol 1. Jayyed, Allahabad (India)Google Scholar
  2. 2.
    Salikutty J, Peter KV (1985) Economy Botany, pp 68–73Google Scholar
  3. 3.
    Verghese J (1989) Perfumer & Flavorist 14:69–70Google Scholar
  4. 4.
    Joseph P, Peter KV, Gopalakrishnan PK (1981) Indian Horticulture, pp 2 and 27Google Scholar
  5. 5.
    Deshmukh SK, Jain PC, Agrawal SC (1986) Fitotherapial LVII, 295–297Google Scholar
  6. 6.
    Patel VK, Venkatakrishna-Bhatt H (1988) Int J of Clinical Pharmacology, Therapy and Toxicology 26:176–184Google Scholar
  7. 7.
    Kureel SP, Kapil RS, Popli SP (1969) Experientia 25:790Google Scholar
  8. 8.
    Chakraborty DP, Islam A, Basak SP, Das R (1970) Chemistry and Industry, p 593Google Scholar
  9. 9.
    Bordner J, Chakraborty DP, Chowdhury BK, Ganguli SN, Das KC, Weinstein B (1972) Experientia 28:1406Google Scholar
  10. 10.
    Roy S, Chakraborty DP (1974) Phytochemistry 13:2893Google Scholar
  11. 11.
    Chakraborty DP, Bhattacharyya P, Islam A, Roy S (1974) Chemistry and Industry, p 165Google Scholar
  12. 12.
    Chakraborty DP, Bhattacharyya P, Mitra AR (1974) Chemistry and Industry, p 260Google Scholar
  13. 13.
    Narasimhan NS, Kelkar SL (1976) Indian J Chem 14B:430Google Scholar
  14. 14.
    Chakraborty DP, Bhattacharyya P, Roy S, Bhattacharyya SP, Biswas AK (1978) Phytochemistry 17:834–835Google Scholar
  15. 15.
    Rama Rao AV, Bhide KS, Mujumdar RB (1980) Chemistry and Industry, p 697Google Scholar
  16. 16.
    Mukherjee M, Mukherjee S, Shaw AK, Ganguly SN (1983) Phytochemistry 22:2328Google Scholar
  17. 17.
    Bhattacharyya P, Chowdhury BK (1985) Indian J Chem 24B:452Google Scholar
  18. 18.
    Fiebig M, Pezzuto JM, Soejarto DD, Kinghorn D (1985) Phytochemistry 24:3041Google Scholar
  19. 19.
    Bhattacharyya P, Jash SS, Chowdhury BK (1986) Chemistry and Industry, p 246Google Scholar
  20. 20.
    Kong Yun-Cheng, Kam-Hung Ng, Pui-Hay But P, Qian Li, Si-Xao Yu, Hong-Ta Zhang, Kin-Fai Cheng, Soejarto DD, Woei-Sang Kan, Waterman PG (1986) J Ethnopharmacology 15:195Google Scholar
  21. 21.
    Bhattacharyya P, Chakraborty A (1984) J Indian Chem Soc 61:650Google Scholar
  22. 22.
    Deshmukh SK, Jain PC, Agrawal SC (1986) Fitotherapia LVII:295–297Google Scholar
  23. 23.
    MacLeod AJ, Piris NM (1982) Phytochemistry 21:1653–1657Google Scholar
  24. 24.
    Quan Li, Liang-Feng Zhu, But PP-H, Yun-Cheung Kong, Hung-Ta Chang, Waterman PG (1988) Biochemical Systematics and Ecology 16:491–494Google Scholar
  25. 25.
    Waßmuth-Wagner I (1991) Dissertation, SaarbrückenGoogle Scholar
  26. 26.
    Waßmuth-Wagner I, Jork H (1992) J Planar Chromatogr 5:383–387Google Scholar
  27. 27.
    Morita M, Mihashi S, Itokawa H, Hara S (1983) Fresenius Z Anal Chem 55:412–414Google Scholar
  28. 28.
    Weyerstahl P, Marschall-Weyerstahl H, Christiansen C, Oguntimein BO, Adeoye AO (1988) Planta Medica, pp 546–549Google Scholar
  29. 29.
    Jork H, Funk W, Fischer W, Wimmer H (1989) Dünnschicht-Chromatographie, Reagenzien und Nachweismethoden. VCH, WeinheimGoogle Scholar
  30. 30.
    Speckenbach F (1989) Füllen von Säulen für die präparative MPLC, Referat, Chroma Prep '89, BaselGoogle Scholar
  31. 31.
    Waßmuth-Wagner I, Kalinowski H-O, Jork H (1993) Planta Medica (in press)Google Scholar
  32. 32.
    Kessler H, Gehrke M, Griesinger C (1988) Angew Chem 100:507–554Google Scholar
  33. 33.
    Braunschweiler L, Ernst RR (1983) J Magn Reson 53:521–528Google Scholar

Copyright information

© Springer-Verlag 1993

Authors and Affiliations

  • I. Waßmuth-Wagner
    • 1
  • H.-O. Kalinowski
    • 2
  • H. Jork
    • 1
  1. 1.Universität des Saarlandes, Fachbereich Pharmazie und Biologische ChemieSaarbrückenGermany
  2. 2.Institut für Organische Chemie der Justus-Liebig-UniversitätGießenGermany

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