Skip to main content
Log in

Size and morphology controlling of barium titanate nanocubes by using hydrothermal method

  • Published:
Journal of the Korean Physical Society Aims and scope Submit manuscript

Abstract

Nano-sized barium titanate (BT) cubes were synthesized by using a hydrothermal method with an aqueous Ti compound. tert-Butylamine was used as an activation agent to expedite precursor hydrolysis. Oleic acid was employed as a surfactant. The concentrations of the raw materials were found to have a very important effect on tailoring the size and the morphology of the BT nanocubes. The size of the nanocubes varied from 15 nm to 30 nm, and the size distribution was relatively narrow. The surface condition and the size of the BT nanocubes were related to the molar ratios of oleic acid to tert-butylamine. High molar ratios resulted in BT nanocubes with rough surfaces.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. S. Wada, T. Hoshina, K. Takizawa, M. Ohishi, H. Yasuno, H. Kakemoto, T. Tsurumi, C. Moriyoshi and Y. Kuroiwa, J. Korean Phys. Soc. 51, 878 (2007).

    Article  ADS  Google Scholar 

  2. B. Huybrechts, K. Ishizaki and M. Takata, J. Mater. Sci. 30, 2463 (1995).

    Article  ADS  Google Scholar 

  3. G. J. Choi, S. K. Lee, K. J. Woo, K. K. Koo and Y. S. Cho, Chem. Mater. 10, 4104 (1998).

    Article  Google Scholar 

  4. X. Xing, J. Deng, J. Chen and G. Liu, J. Alloys Compd. 384, 312 (2004).

    Article  Google Scholar 

  5. D. Hennings, M. Klee and R. Waser, Adv. Mater. 3, 334 (1991).

    Article  Google Scholar 

  6. S. Adireddy, C. K. Lin, B. B. Cao, W. L. Zhou and G. Caruntu, Chem. Mater. 22, 1946 (2010).

    Article  Google Scholar 

  7. S. Moon, H. W. Lee, C. H. Choi and D. K. Kim, J. Am. Ceram. Soc. 7, 2248 (2012).

    Article  Google Scholar 

  8. J. Zhou and Z. C. Yang, Cryst. Eng. Comm. 15, 8912 (2013).

    Article  Google Scholar 

  9. W. W. Wang, L. X. Cao, W. Liu, G. Su and W. X. Zhang, Ceram. Inter. 39, 7127 (2013).

    Article  Google Scholar 

  10. J. Adam, G. Klein and T. Lehnert, J. Am. Ceram. Soc. 96, 2987 (2013).

    Article  Google Scholar 

  11. F. Dang, K. Mimura, K. Kato, H. Imai, S. Wada, H. Haneda and M. Kuwabara, Nanoscale. 4, 1344 (2012).

    Article  ADS  Google Scholar 

  12. K. Mimura and K. Kato, APEX 7, 061501 (2014).

  13. K. Kato, K. Mimura, F. Dang, H. Imai, S. Wada, M. Osada H. Haneda and M. Kuwabara, J. Mater. Res. 28, 2932 (2013).

    Article  ADS  Google Scholar 

  14. Q. Ma, K. Mimura and K. Kato, CrystEngComm. 16, 8398 (2014).

    Article  Google Scholar 

  15. T. D. Nguyen and T. O. Do, J. Phys. Chem. C. 113, 11204 (2009).

    Article  Google Scholar 

  16. Y. H. Zheng, Y. M. Tian, H. L. Ma, Y. N. Qu, Z. C. Wang, D. M. An, S. Guan and X. Y. Gao, Colloids Surf. A: Physicochem. Eng. Aspects. 339, 178 (2009).

    Article  Google Scholar 

  17. T. D. Nguyen, C. T. Dinh and T. O. Do, Inorg. Chem. 50, 1309 (2011).

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Qiang Ma.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Ma, Q., Mimura, Ki. & Kato, K. Size and morphology controlling of barium titanate nanocubes by using hydrothermal method. Journal of the Korean Physical Society 66, 1364–1366 (2015). https://doi.org/10.3938/jkps.66.1364

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.3938/jkps.66.1364

Keywords

Navigation