Abstract
Maghemite nanoparticles of 40 to 150 nm are obtained by the thermal decomposition of preliminarily cryochemically modified iron acetylacetonate. The composition and structure of the obtained particles and cryomodified precursor salt are determined by the X-ray diffraction (XRD) analysis, thermoanalytical methods (thermogravimetry, differential scanning calorimetry), infrared spectroscopy, and transmission electron microscopy.
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REFERENCES
Hwang, S., Umar, A., Dar, G., Kim, S.H., and Badran, R., Sensor Appl.Sensor Lett., 2014, vol. 5, p. 97.
Long, N.V., Teranishi, T., Yang, Y., Thi, C., Cao, Y., and Nogami, M., Int. J. Metall. Mater. Eng., 2015, vol. 1, p. 119.
Vallabani, N.V.S. and Singh, S., Biotech, 2018, vol. 8, p. 279.
Fu, C. and Ravindra, N., Bioinspired,Biomimetic Nanobiomater., 2012, vol. 1, no. 4, p. 229.
Leong, S.S., Yeap, S.P., and Lim, J.K., Interface Focus, 2016, vol. 6, no. 6, 20160048.
Sumpter, B.G., Dave, P.N., and Chopda, L.V., J. Nanotech., 2014, 398569. https://www.hindawi.com/journals/ jnt/2014/398569.
Arias, L.S., Pessan, J.P., Vieira, A.P.M., Lima, T.M.T., Delbem, A.C.B., and Monteiro, D.R., Antibiotics (Basel, Switz.), 2018, vol. 7, no. 2, p. 46
Ansari, S.A.M.K., Ficiara, E., Ruffinatti, F.A., Stura, I., Argenziano, M., Abollino, O., Cavalli, R., Guiot, C., and D’Agata, F., Materials (Basel, Switz.), 2019, vol. 12, no. 3, p. 465.
Rostovshchikova, T.N., Smirnov, V.V., Tsodikov, M.V., Bukhtenko, O.V., and Maksimov, Yu.V., Kiseleva, O.I., Pankratov, D.A, Russ. Chem. Bull., 2005, vol. 54, p. 1418.
Rostovshchikova, T., Smirnov, V., Kiseleva, O., Yushcenko, V., Tzodikov, M., Maksimov, Y., Suzdalev, I., Kustov, L., and Tkachenko, O., Catal. Today, 2010, vol. 152, nos. 1–4, p. 48.
Moodley, P., Scheijen, F.J.E., Niemantsverdriet, J.W., and Thune, P.C., Catal. Today, 2010, vol. 154, nos. 1–2, p. 142.
Hugounenq, P., Levy, M., Alloyeau, D., Lartigue, L., Dubois, E., Cabuil, V., Ricolleau, C., Roux, S., Wilhelm, C., Gazeau, F., and Bazzi, R., J. Phys. Chem. C, 2012, vol. 116, p. 15702.
Kurland, H.-D., Grabow, J., Staupendahl, G., Müller, F.A., Müller, E., Dutz, S., and Bellemann, M.E., J. Magn. Magn. Mater., 2009, vol. 321, p. 1381.
Kurland, H.-D., Grabow, J., Dutz, S., Müller, E., Sierka, M., and Müller, F.A., Cryst. Growth Des., 2013, vol. 13, p. 4868.
Timko, M., Molcan, M., Hashim, A., Skumiel, A., Müller, M., Gojzewski, H., Jozefczak, A., Kovac, J., Rajnak, M., Makowski, M., and Kopčanský, P., IEEE Trans. Magn., 2013, vol. 49, p. 250.
McBain, S., Yiu, H., and Dobson, J., Int. J. Nanomed., 2008, vol. 3, p. 169.
Shabatina, T.I., Vernaya, O.I., Nuzhdina, A.V., Zvukova, N.D., Semenov, A.M., Shabatin, V.P., Lozinskii, V.I., and Mel’nikov, M.Ya., Nanotechnol. Russ., 2018, vol. 13, p. 182.
Shabatina, T.I., Vernaya, O.I. Karlova, D.L., Nuzhdina, A.V., Shabatin, V.P., Semenov, A.M., Lozinskii, V.I., and Mel’nikov, M.Ya., Nanotechnol. Russ., 2018, vol. 13, p. 546.
Vernaya, O.I., Shabatin, V.P., Semenov, A.M., Shabatina, T.I., and Mel’nikov, M.Ya., Moscow Univ. Chem. Bull. (Engl. Transl.), 2020, vol. 75, no. 4, p. 258.
Shabatina, T.I., Vernaya, O.I., Shabatin, V.P., Melnikov, M.Y., Semenov, A.M., and Lozinsky, V.I., Appl. Sci., 2020, vol. 10, no. 1, 170.
Diaz-Acosta, D., Baker, J., Cordes, W., and Pulay, P., J. Phys. Chem. A, 2001, vol. 105, p. 238.
Cornell, R.M. and Schwertmann, U., The Iron Oxides: Structure, Properties, Reactions, Occurrences and Uses, New York: Wiley, 2003, p. 147.
Kolida, Yu.Ya., Antonova, A.S., Kropacheva, T.N., and Kornev, V.I., Vestn. Udmurt. Univ., 2014, no. 4, p. 52.
Kim, W., Suh, C.-Y., Cho, S.-W., Roh, K.-M., Kwon, H., Song, K., and Shon, I.-J., Talanta, 2012, vol. 94, p. 348.
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This work was supported by the Russian Science Foundation (project no. 16-13-10365-П).
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Translated by E. Boltukhina
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Vernaya, O.I., Shumilkin, A.S., Shabatin, V.P. et al. The Synthesis of Maghemite Nanoparticles by Thermal Decomposition of Cryochemically Modified Iron(III) Acetylacetonate. Moscow Univ. Chem. Bull. 75, 265–268 (2020). https://doi.org/10.3103/S0027131420050089
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DOI: https://doi.org/10.3103/S0027131420050089