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Laser-Induced Breakdown Spectrometry for Analyzing the Composition of the Products during Coaxial Laser Cladding

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Moscow University Chemistry Bulletin Aims and scope

Abstract

We demonstrate the possibility of the quantitative multielement analysis of a composite wear-resistant coating (tungsten carbide particles in chromium–nickel matrix) during its synthesis by coaxial laser cladding. The developed probe for the laser-induced breakdown spectrometry (LIBS) was used for the online analysis of the concentration of carbon, tungsten, and nickel in the process of applying a wear-resistant coating. The results of online LIBS measurements agreed closely with the results of the offline analyses using conventional methods such as X-ray fluorescence spectrometry, X-ray spectral electron probe microanalysis, and the combustion infrared absorption method using a LECO gas analyzer.

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Funding

This work was supported by the Russian Science Foundation, project no. 16-19-10656.

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Authors and Affiliations

  1. Prokhorov General Physics Institute, Russian Academy of Sciences, 119991, Moscow, Russia

    P. A. Sdvizhenskii, V. N. Lednev, M. Ya. Grishin & S. M. Pershin

  2. National University of Science and Technology MiSiS, 119049, Moscow, Russia

    P. A. Sdvizhenskii & V. N. Lednev

  3. Bauman Moscow State Technical University, 105005, Moscow, Russia

    R. D. Asyutin

  4. Moscow Institute of Physics and Technology (National Research University), 141701, Dolgoprudny, Moscow oblast, Russia

    M. Ya. Grishin

Authors
  1. P. A. Sdvizhenskii
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  2. V. N. Lednev
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  3. R. D. Asyutin
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  4. M. Ya. Grishin
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  5. S. M. Pershin
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Corresponding author

Correspondence to P. A. Sdvizhenskii.

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The authors declare that they have no conflict of interest.

Additional information

Translated by O. Zhukova

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Sdvizhenskii, P.A., Lednev, V.N., Asyutin, R.D. et al. Laser-Induced Breakdown Spectrometry for Analyzing the Composition of the Products during Coaxial Laser Cladding. Moscow Univ. Chem. Bull. 75, 77–81 (2020). https://doi.org/10.3103/S0027131420020133

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  • DOI: https://doi.org/10.3103/S0027131420020133

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