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Application of microemulsions for the extraction of o-phthalate esters from soil with subsequent separation of microemulsions, simultaneous preconcentration, and gas chromatographic analysis of target components

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Abstract

The possible application of microemulsions as extractants for the extraction of o-phthalate esters from soils with the subsequent breakdown of microemulsions, simultaneous preconcentration of dialkhylphthalates in the organic phase, and their following gas chromatographic analysis with mass-spectrometric detection is demonstrated. The preconcentration factor was 18. The method is characterized by low detection limits, good selectivity, and reproducibility.

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Authors and Affiliations

  1. Chemistry Department, Moscow State University, Moscow, Russia

    N. G. Tolmacheva, A. V. Pirogov & O. A. Shpigun

Authors
  1. N. G. Tolmacheva
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  2. A. V. Pirogov
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  3. O. A. Shpigun
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Corresponding author

Correspondence to N. G. Tolmacheva.

Additional information

Original Russian Text © N.G. Tolmacheva, A.V. Pirogov, O.A. Shpigun, 2017, published in Vestnik Moskovskogo Universiteta, Seriya 2: Khimiya, 2017, No. 2, pp. 83–88.

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Tolmacheva, N.G., Pirogov, A.V. & Shpigun, O.A. Application of microemulsions for the extraction of o-phthalate esters from soil with subsequent separation of microemulsions, simultaneous preconcentration, and gas chromatographic analysis of target components. Moscow Univ. Chem. Bull. 72, 92–96 (2017). https://doi.org/10.3103/S0027131417020043

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  • DOI: https://doi.org/10.3103/S0027131417020043

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