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On-line solid-phase extraction and HPLC determination of phthalic acid monoesters including desorption with subcritical water

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Abstract

The possibility of on-line solid-phase extraction and HPLC determination of phthalic acid monoesters is demonstrated. The combined procedure includes solid-phase extraction of phthalates from 10 mL of water on a Hypercarb porous graphitic carbon sorbent, desorption with subcritical water at 150°C, focusing of the analytes at the initial part of the HPLC column, and separation with a water–acetonitrile mixture.

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Authors and Affiliations

  1. Department of Chemistry, Moscow State University, Moscow, 119991, Russia

    D. R. Borisova, E. N. Goncharova, M. A. Statkus & G. I. Tsisin

Authors
  1. D. R. Borisova
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  2. E. N. Goncharova
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  3. M. A. Statkus
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  4. G. I. Tsisin
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Corresponding author

Correspondence to D. R. Borisova.

Additional information

Original Russian Text © D.R. Borisova, E.N. Goncharova, M.A. Statkus, G.I. Tsisin, 2015, published in Vestnik Moskovskogo Universiteta. Khimiya, 2015, No. 5, pp. 296–301.

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Borisova, D.R., Goncharova, E.N., Statkus, M.A. et al. On-line solid-phase extraction and HPLC determination of phthalic acid monoesters including desorption with subcritical water. Moscow Univ. Chem. Bull. 70, 237–241 (2015). https://doi.org/10.3103/S002713141505003X

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  • DOI: https://doi.org/10.3103/S002713141505003X

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