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Ceramics Based on Powders Synthesized from Ammonium Hydrogen Phosphate, Calcium Acetate, and Magnesium Acetate

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Inorganic Materials: Applied Research Aims and scope

Abstract

A ceramic the phase composition of which included tricalcium phosphate, calcium magnesium orthophosphate, and magnesium pyrophosphate was prepared from nanosized powders synthesized via chemical deposition from 1 M aqueous solutions of ammonium hydrogen phosphate and calcium and/or magnesium acetates. The XRD data showed that the phase composition of a powder synthesized from calcium acetate involved calcium hydroxyapatite Ca5(PO4)3(OH), octacalcium phosphate Ca8H2(PO4)6⋅5H2O, and brushite CaHPO4⋅2H2O. The phase composition of a powder synthesized from magnesium acetate included struvite MgNH4PO4⋅6H2O. The phase composition of a powder synthesized from a solution containing calcium and magnesium acetates at a Ca : Mg ratio of 9 : 1 included hydroxyapatite Ca5(PO4)3(OH), vitlockite Ca18Mg2H2(PO4)14, and struvite MgNH4PO4⋅6H2O. The ceramic materials containing bioresorbable and biocompatible phases of calcium and/or magnesium phosphates can be used to obtain bone implants for the treatment of bone tissue defects.

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ACKNOWLEDGMENTS

This work was performed with use of equipment acquired at the expense of the Program of Development of Moscow University.

Funding

This work was financially supported by the Russian Foundation for Basic Research (project 19-38-90274).

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Authors and Affiliations

  1. Moscow State University, 119991, Moscow, Russia

    G. K. Kazakova, T. V. Safronova & T. B. Shatalova

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  1. G. K. Kazakova
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  2. T. V. Safronova
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  3. T. B. Shatalova
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Correspondence to G. K. Kazakova.

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Translated by A. Tulyabaew

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Kazakova, G.K., Safronova, T.V. & Shatalova, T.B. Ceramics Based on Powders Synthesized from Ammonium Hydrogen Phosphate, Calcium Acetate, and Magnesium Acetate. Inorg. Mater. Appl. Res. 13, 75–82 (2022). https://doi.org/10.1134/S2075113322010154

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