Skip to main content
Log in

Composite Material Based on Intermetallic Alloy of VKNA Type Reinforced with Oxide Particles

  • MATERIALS OF AIRCRAFT AND AEROSPACE ENGINEERING
  • Published:
Inorganic Materials: Applied Research Aims and scope

Abstract

The technology of obtaining composite material experimental samples based on an intermetallic alloy of VKNA type reinforced with oxide particles in an amount of 2–5 vol % is presented. An intermetallic VKNA-1V alloy containing 80–90 wt % of γ' phase was used as the matrix prototype. Al2O3 particles, as well as complex oxides AI2O3⋅Y2O3, AI2O3⋅Y2O3⋅HfO2, were used as reinforcing particles. Granules of VKNA-1V alloy were obtained by gas atomization at the Hermiga Gas Atomiser. Subsequently, these granules were subjected to mechanical alloying with the aim of introducing particles of the aforementioned compositions of oxides to form a composite mixture corresponding in composition to the desired composite material. Experimental composite material samples with different contents of reinforcing particles were obtained from powder mixtures by spark plasma sintering (SPS) with further hot isostatic pressing (HIP). To study the microstructure of experimental samples, the method of scanning electron microscopy was used. Time to failure of experimental samples sintered by spark plasma combined with HIP was determined at a temperature of 900°С and stress of 50, 45, and 35 MPa. It is shown that to determine the areas of application of the developed composition, the hot isostatic pressing operation is necessary, but not sufficient.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1.
Fig. 2.
Fig. 3.
Fig. 4.
Fig. 5.

Similar content being viewed by others

REFERENCES

  1. Kablov, E.N., Innovative Developments of FSUE “VIAM” SSC of RF on realization of “Strategic Directions of the Development of Materials and Technologies of Their Processing for the Period Until 2030”, Aviats. Mater. Tekhnol., 2015, no. 1 (34), pp. 3–33. https://doi.org/10.18577/2071-9140-2015-0-1-3-33

  2. Kablov, E.N., Strategical areas of developing materials and their processing technologies for the period up to 2030, Aviats. Mater. Tekhnol., 2012, no. S, pp. 7–17.

  3. Kablov, E.N., VIAM: Materials of new generation for PD-14, Kryl’ya Rodiny, 2019, nos. 7–8, pp. 54–58.

  4. Burkovskaya, N.P., Efimochkin, I.Yu., Bazyleva, O.A., et al., Study of structural features, strength properties, and heat resistance of a dispersion-hardened composite material based on nickel intermetallide, Inorg. Mater.: Appl. Res., 2016, vol. 7, pp. 603–609. https://doi.org/10.1134/S2075113316040079

    Article  Google Scholar 

  5. Rodionov, A.I., Bolshakova, A.N., and Efimochkin, I.Yu., Study of the influence of the nature and concentration of oxide reinforcing filler on strength characteristics of the VKNA-4U alloy, Perspekt. Mater., 2017, no. 12, pp. 18–25.

  6. Trofimenko, N.N., Efimochkin, I.Yu., and Bolshakova, A.N., Problems of creation and prospects for the use of heat-resistant high-entropy alloys, Aviats. Mater. Tekhnol., 2018, no. 2 (51), pp. 3–8. https://doi.org/10.18577/2071-9140-2018-0-2-3-8

  7. Grashchenkov, D.V., Efimochkin, I.Yu., and Bolshakova, A.N., High-temperature metal-matrix composite materials reinforced with particles and fibers of refractory compounds, Aviats. Mater. Tekhnol., 2017, no. S, pp. 318–328. https://doi.org/10.18577/2071-9240-2017-0-S-318-328

  8. Bolshakova, A.N., Efimochkin, I.Yu., and Mura-sheva, V.V., Mechanically alloyed dispersion-strengthened composite materials, Konstr. Kompoz. Mater., 2015, no. 1 (137), pp. 36–40.

  9. Shchetanov, B.V., Grashchenkov, D.V., Efimochkin, I.Yu., and Shcheglova, T.M., Monocrystalline aluminum oxide fibers for high-temperature (up to 1400°C) composite materials, Tekhnol. Mashinostr., 2014, no. 10, pp. 5–9.

  10. Efimochkin, I.Yu., Kuptsov, R.S., Arginbaeva, E.G., Bazyleva, O.A., Grashchenkov, D.V., and Kablov, E.N., Patent RF no. 0002686831, declared 22.03.2018, published 30.04.2019.

  11. Evgenov, A.G., Afanas’ev-Khodykin, A.N., Nerush, S.V., and Rogalev, A.M., Metallurgical aspects of production of solder powders for vacuum diffusion brazing, Metallurgist, 2014, vol. 57, nos. 11–12, pp. 1120–1125. https://doi.org/10.1007/s11015-014-9855-9

  12. Rogalev, A.M., Shcherbakov, A.I., Afanasyev-Khodykin, A.N., Nerush, S.V., Evgenov, A.G., and Kablov, E.N., Patent RF no. 2492028, declared 02.07.2012, published 10.09.2013.

  13. Kotlyarov, V.I., Beshkarev, V.T., Kartsev, V.E., Ivanov, V.V., Gasanov, A.A., Yuzhakova, E.A., Samokhin, A.V., Fadeev, A.A., Alekseev, N.V., Sinayskiy, M.A., and Tretyakov E.V., Production of spherical powders on the basis of group IV metals for additive manufacturing, Inorg. Mater.: Appl. Res., 2017, vol. 8, pp. 452–458. https://doi.org/10.1134/S2075113317030157

    Article  Google Scholar 

  14. Tsvetkov, Yu.V., Samokhin, A.V., Fadeev, A.A., Alekseev, N.V., and Kotlyarov, V.I., Spheroidizing of metal powders in thermal dc plasma, Tekhnol. Legkikh Splavov, 2016, no. 2, pp. 19–24.

  15. Grashchenkov, D.V., Evdokimov, S.A., Zhestkov, B.E., Solntsev, S.S., and Shtapov, V.V., Research of thermochemical influence of the air plasma flow on high-temperature ceramic composite material, Aviats. Mater. Tekhnol., 2017, no. 2 (47), pp. 31–40. https://doi.org/10.18577/2071-9140-2017-0-2-31-40

  16. Grashchenkov, D.V., Prospects for the use of spark plasma sintering for the creation of high-temperature composite materials, Proc. 2nd Sci. Tech. Conf. “High-Temperature Ceramic Composite Materials and Protective Coatings”, Moscow: VIAM, 2016, p. 5.

  17. Ospennikova, O.G., Kalitcev, V.A., Yevgenov, A.G., and Bazyleva, O.A., Integration of hot isostatic pressing with temperature treatment of polycrystalline moldings from alloy based on intermetalloid Ni3Al, Vestn. MGTU im. N.E. Baumana, Ser. Mashinostr., 2011, no. S2, pp. 88–97. https://www.elibrary.ru/item.asp?id=17849069.

Download references

ACKNOWLEDGMENTS

This work was carried out within the framework of the implementation of the complex discipline 7.3 “Intermetallic Nickel Alloys and Composites Based on Them” and 12 “Metal Matrix and Polymatrix Composite Materials” (“Strategic Directions for the Development of Materials and Technologies for Their Processing for the Period up to 2030”) [12].

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to O. A. Bazyleva.

Additional information

Translated by M. Drozdova

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Bazyleva, O.A., Efimochkin, I.Y., Arginbaeva, E.G. et al. Composite Material Based on Intermetallic Alloy of VKNA Type Reinforced with Oxide Particles. Inorg. Mater. Appl. Res. 12, 307–312 (2021). https://doi.org/10.1134/S2075113321020088

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S2075113321020088

Keywords:

Navigation