Skip to main content
SpringerLink
Log in

Methodological Aspects of Determining Fiber—Matrix Adhesive Strength by Pushing out Monofilament with an Indenter

  • Published:
Polymer Science, Series D Aims and scope Submit manuscript

Abstract

The results of determining the fiber–matrix adhesive strength by the method of pushing out a monofilament with an indenter for various grades of carbon fiber plastics have been presented. The factors influencing the correctness of obtaining experimental data have been considered. It has been shown that the fiber–matrix adhesive strength determined by this method can be considered as a size-independent quantity.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1.
Fig. 2.
Fig. 3.
Fig. 4.

Similar content being viewed by others

REFERENCES

  1. A. E. Raskutin, “Strategy for the development of polymer composite materials,” Aviats. Mater. Tekhnol., No. S, 344–348 (2017). https://doi.org/10.18577/2071-9140-2017-0-S-344-348

  2. E. N. Kablov, M. I. Valueva, I. V. Zelenina, V. V. Khmelnitsky, and V. M. Aleksashin, “Carbon plastics based on benzoxazine oligomers–promising materials,” Trudy VIAM, No. 1, 68–77 (2020). https://doi.org/10.18577/2307-6046-2020-0-1-68-77

  3. E. N. Kablov, L. V. Chursova, N. F. Lukina, K. E. Kutsevich, E. V. Rubtsova, and A. P. Petrova, “Study of epoxy-polysulfone polymer systems as the basis for high-strength aviation adhesives,” Klei. Germetiki. Tekhnol., No. 3. P. 7–12 (2017).

  4. E. N. Kablov, G. S. Kulagina, G. F. Zhelezina, S. L. Lonsky, and E. V. Kurshev, “Study of the microstructure of unidirectional organoplastic based on Rusar-NT aramid fibers and epoxy-polysulfone binder,” Aviats. Mater. Tekhnol., No. 4, 19–26 (2020). https://doi.org/10.18577/2071-9140-2020-0-4-19-26

  5. P. G. Belinis, K. I. Donetsky, Yu. V. Lukyanenko, V. N. Rogozhnikov, Yu. Mayer, and D. V. Bystrikova, “Volume-reinforcing seamless preforms for the manufacture of polymer composite materials (review),” Aviats. Mater. Tekhnol., No. 4, 18–26 (2019). https://doi.org/10.18577/2071-9140-2019-0-4-18-26

  6. A. I. Sidorina, “Modification of the surface of carbon reinforcing fillers for polymer composite materials by electrochemical processing (review),” Trudy VIAM, No. 4, 07 (2022). https://doi.org/10.18577/2307-6046-2022-0-4-61‑74

  7. A. R. Garifullin and I. Sh. Abdullin, “Current state of the problem of surface treatment of carbon fibers for their subsequent use in polymer composites as a reinforcing element,” Vestn. Kazan Tekhnol. Univ., No. 7, 80–85 (2014).

  8. J. Karger-Kocsis, H. Mahmood, and A. Pegoretti, “Recent advances in fiber/matrix interphase engineering for polymer composites,” Prog. Mater. Sci. 73, 1–43 (2015).

    Article  CAS  Google Scholar 

  9. J. D. H. Hughes, “The carbon fibre/epoxy interface–a review,” Compos. Sci. Technol. 41, 13–45 (1991).

    Article  CAS  Google Scholar 

  10. J.-K. Kim and Y.-W. Mai, Engineered Interfaces in Fiber Reinforced Composites (Elsevier, Oxford, 1998).

    Google Scholar 

  11. V. A. Nelyub and P. A. Belov, “Methods for increasing the resistance of carbon fiber plastics to delamination by controlling the adhesion of the fiber to the matrix,” Nov. Mater. Nauka Tekh., No. 5, 3 (2013).

  12. M. Nardin and J. Schultz, “Relationship between fibre-matrix adhesion and the interfacial shear strength in polymer-based composites,” Compos. Interfaces 1, 177–192 (1993).

    Article  CAS  Google Scholar 

  13. R. Plonka, E. Mader, S. L. Gao, C. Bellmann, V. Dutschk, and S. Zhandarov, “Adhesion of epoxy/glass fibre composites influenced by aging effects on sizings,” Composites, Part A 35, 1207–1216 (2004).

    Article  Google Scholar 

  14. T. Yang, Y. Zhao, H. Liu, M. Sun, and S. Xiong, “Effect of sizing agents on surface properties of carbon fibers and interfacial adhesion of carbon fiber/bismaleimide composites,” ACS Omega 6, 23028–23037 (2021).

    Article  CAS  PubMed  PubMed Central  Google Scholar 

  15. Yu. A. Gorbatkina, Adhesive Strength in Polymer-Fiber Systems (Khimiya, Moscow, 1987) [in Russian].

    Google Scholar 

  16. O. V. Akhmatova, Yu. A. Gorbatkina, I. Yu. Gorbunova, V. G. Ivanova-Mumzhieva, and M. L. Kerber, “The influence of nano-sized clay particles and thermoplastic modifier on the adhesive strength of epoxyamine binder compounds with fibers,” Plast. Massy, No. 10, 31–35 (2012).

    Google Scholar 

  17. Yu. A. Gorbatkina, V. G. Ivanova-Mumzhieva, and A. M. Kuperman, “Adhesion of modified epoxy matrices to reinforcing fibers,” Polym. Sci., Ser. A 58, 659–666 (2016)

    Article  CAS  Google Scholar 

  18. A. Yu. Sergeev, R. A. Turusov, and N. I. Baurova, “Determination of the adhesive strength of joints using the example of testing samples by pulling fibers out of the matrix,” Kompoz. Nanostruktury, No. 1, 52–62 (2017).

    Google Scholar 

  19. A. S. Borodulin, V. V. Mal’tsev, A. A. Bertaeva, S. Yu. Fedorov, A. G. Tereshkov, V. A. Nelyub, and G. V. Malysheva, “Methodology for assessing the adhesive strength of an elementary fiber-epoxy matrix system,” Klei. Germetiki. Tekhnol., No. 5, 32–38 (2022).

  20. Z. Dai, F. Shi, B. Zhang, M. Li, and Z. Zhang, “Effect of sizing on carbon fiber surface properties and fibers/epoxy interfacial adhesion,” Appl. Surf. Sci. 257 6980–6985 (2011).

    Article  CAS  Google Scholar 

  21. S. Tamrakar, B. Z. Haque (Gama), and J. W. Gillespie, “High rate test method for fiber-matrix interface characterization,” Polym. Test. 52, 174–183 (2016).

    Article  CAS  Google Scholar 

  22. A. I. Gulyaev, “Measuring fiber-matrix adhesive strength using nanoindentation (review),” Trudy VIAM, No. 3, 08 (2019). https://doi.org/10.18577/2307-6046-2019-0-3-8-8

  23. Yu. I. Golovin, “Nanoindentation and mechanical properties of materials at submicro- and nanoscale levels: recent results and achievements,” Phys. Solid State 63, 1–41 (2021).

    Article  CAS  Google Scholar 

  24. J. M. Molina-Aldareguia, M. Rodriguez, C. Gonzalez, and J. Lorca, “An experimental and numerical study of the influence of local effects on the application of the fibre push-in test,” Phil. Mag. 91, 1293–1307 (2011).

    Article  CAS  Google Scholar 

  25. A. Godara, L. Gorbatikh, G. Kalinka, A. Warrier, O. Rochez, L. Mezzo, F. Luizi, A. W. van Vuure, S. V. Lomov, and I. Verpoest, “Interfacial shear strength of a glass fiber/epoxy bonding in composites modified with carbon nanotubes,” Compos. Sci. Technol. 70, 1346–1352 (2010).

    Article  CAS  Google Scholar 

  26. J. Jager, M. G. R. Sause, F. Burkert, J. Moosburger-Will, M. Greisel, and S. Horn, “Influence of plastic deformation on single-fiber push-out tests of carbon fiber reinforced epoxy resin,” Composites, Part A 71, 157–167 (2015).

    Article  Google Scholar 

  27. S. C. Gallo, X. Li, Z. Zhang, C. Charitidis, and H. Dong, “Viscoelastic response of carbon fibre reinforced polymer during push-out tests,” Composites, Part A 112, 178–185 (2018).

    Article  Google Scholar 

  28. A. I. Gulyaev, P. N. Medvedev, S. V. Sbitneva, and A. A. Petrov, “Experimental study to assess the adhesive strength of fiber-matrix in carbon fiber reinforced plastics based on epoxy binder modified with polysulfone,” Aviats. Mater. Tekhnol., No. 4, 80–86 (2019). https://doi.org/10.18577/2071-9140-2019-0-4-80-86

  29. A. Ya. Gorenberg, Yu. A. Gorbatkina, and V. G. Ivanova-Mumzhieva, “Evaluation of interfacial strength during adhesion of polymers to fibers with a rough surface,” Klei. Germetiki. Tekhnol., No. 3, 36–41 (2021).

Download references

ACKNOWLEDGMENTS

The work was carried out using the equipment of the “Climate Tests” Center for Collective Use of Federal State Unitary Enterprise “All-Russian Research Institute of Aviation Materials” of the National Research Center “Kurchatov Institute”

Funding

This work was supported by ongoing institutional funding. No additional grants to carry out or direct this particular research were obtained.

Author information

Authors and Affiliations

  1. Federal State Unitary Enterprise “All-Russian Research Institute of Aviation Materials,” National Research Center “Kurchatov Institute”, 105005, Moscow, Russia

    A. I. Gulyaev, S. V. Sbitneva, D. V. Zaitsev & P. N. Medvedev

Authors
  1. A. I. Gulyaev
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. S. V. Sbitneva
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. D. V. Zaitsev
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. P. N. Medvedev
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to A. I. Gulyaev.

Ethics declarations

The authors of this work declare that they have no conflicts of interest.

Additional information

Translated by Sh. Galyaltdinov

Publisher’s Note.

Pleiades Publishing remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Gulyaev, A.I., Sbitneva, S.V., Zaitsev, D.V. et al. Methodological Aspects of Determining Fiber—Matrix Adhesive Strength by Pushing out Monofilament with an Indenter. Polym. Sci. Ser. D 16, 875–881 (2023). https://doi.org/10.1134/S1995421223040123

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S1995421223040123

Keywords:

Search

Navigation