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Recrystallization of Zinc Oxide in a Sub- and Supercritical Water Medium

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Abstract—Electron microscopy was used to study the formation of a dispersed composition of a fine-crystalline powder during the recrystallization of zinc oxide in a water medium at 100–400°C. It was shown that recrystallization in condensed water is difficult but proceeds in a water medium in a vapor or supercritical state in the presence of an activator (ammonium chloride). It occurs under the influence of an introduced activator at temperatures up to 300°C and under the combined influence of the activator and thermal activation of the surface layer of crystals in the range of 300–400°C. In the recrystallization process, monodisperse ZnO powder with an average crystal size of 0.184 μm is converted into a polydisperse powder with several size-distribution components and average sizes from 0.08 to a few μm.

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  1. Chemistry Faculty, Moscow State University, 119991, Moscow, Russia

    Yu. D. Ivakin, M. N. Danchevskaya & G. P. Muravieva

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  1. Yu. D. Ivakin
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Translated by O. Kadkin

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Ivakin, Y.D., Danchevskaya, M.N. & Muravieva, G.P. Recrystallization of Zinc Oxide in a Sub- and Supercritical Water Medium. Russ. J. Phys. Chem. B 13, 1189–1200 (2019). https://doi.org/10.1134/S199079311907011X

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