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Development of a Novel Thermal Resistant Polysulfide/Carbon Fiber Semi-Crystalline Composite

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Abstract

In the current study, a thermal resistant polysulfide composite was prepared by the incorporation of carbon fibers (CFs). Poly(ethylene tetrasulfide) (PETS) was used as the polysulfide matrix as is the most efficient in terms of productivity. The preparation of the PETS/CF composite was conducted via in situ polymerization. Different loading weight percentages (0.5, 1.0, and 2.0) of CF were incorporated into the PETS matrix. The morphology and structural properties of PETS/CF composites were assessed by scanning electron microscopy (SEM), X-ray diffraction (XRD) methods, and Fourier transform infrared (FTIR) technique. In addition, the thermal properties of the composites were examined utilizing differential calorimetry scanning (DSC) and thermogravimetric analysis (TGA) methods. Finally, the effect of incorporation of CF on the chemical resistance of samples was investigated using various solvents. The characterization results showed the successful preparation of the composites. Moreover, the thermal analysis confirmed the significant efficacy of the introducing of CF to the PETS matrix. Furthermore, PETS/CF composites showed a great resistance to different solvents which helps with hindering the solvents transmission within the PETS matrix.

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Author information

Authors and Affiliations

  1. Department of Chemistry, Amirkabir University of Technology, Tehran, Iran

    Mohamadreza Shakiba & Majid Abdouss

  2. Center for Nanotechnology and Sustainability, Department of Mechanical Engineering, Faculty of Engineering, National University of Singapore, 117581, Singapore, Singapore

    Erfan Rezvani Ghomi & Seeram Ramakrishna

  3. Department of Polymer Engineering, Tehran South Branch, Islamic Azad University, Tehran, Iran

    Mohammadreza Kalaee & Ali Khatib

  4. Nanotechnology Research Centre, Tehran South Branch, Islamic Azad University, Tehran, Iran

    Mohammadreza Kalaee

  5. Department of Chemistry, Shahre-Qods Branch, Islamic Azad University, Shahre-Qods, Iran

    Omid Moradi

Authors
  1. Mohamadreza Shakiba
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  2. Erfan Rezvani Ghomi
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  3. Mohammadreza Kalaee
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  4. Majid Abdouss
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  5. Ali Khatib
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  6. Omid Moradi
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  7. Seeram Ramakrishna
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Contributions

Conceptualization: Mohamadreza Shakiba, Mohammadreza Kalaee, Majid Abdouss, Ali Khatib; Methodology: Mohamadreza Shakiba, Mohammadreza Kalaee, Majid Abdouss, Ali Khatib; Validation: Mohamadreza Shakiba, Mohammadreza Kalaee, Majid Abdouss, Ali Khatib; Investigation: Mohamadreza Shakiba, Erfan Rezvani Ghomi, Mohammadreza Kalaee, Majid Abdouss, Ali Khatib; Writing—original draft preparation: Mohamadreza Shakiba, Erfan Rezvani Ghomi, Ali Khatib; Writing—review and editing: Mohamadreza Shakiba, Erfan Rezvani Ghomi, Mohammadreza Kalaee, Majid Abdouss, Seeram Ramakrishna; Supervision: Mohammadreza Kalaee, Majid Abdouss, Seeram Ramakrishna. All authors have read and agreed to the published version of the manuscript.

Corresponding authors

Correspondence to Erfan Rezvani Ghomi or Mohammadreza Kalaee.

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Mohamadreza Shakiba, Ghomi, E.R., Kalaee, M. et al. Development of a Novel Thermal Resistant Polysulfide/Carbon Fiber Semi-Crystalline Composite. Polym. Sci. Ser. B 63, 591–597 (2021). https://doi.org/10.1134/S1560090421050122

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