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Multipurpose synchrotron spectrometer of the Kurchatov Institute: Part 3. Diffraction in Debye–Scherrer geometry

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Abstract

The performance of a multipurpose synchrotron spectrometer is diversified by installing additional equipment for the studies of diffraction in the Debye–Scherrer geometry. The design of X-ray optics and technical characteristics of the spectrometer are described. Diffraction patterns for polycrystals detected in both the forward and backward hemispheres are illustrated.

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References

  1. www.esrf.eu/home/UsersAndScience/Experiments/Beamlines/content/content/ID22.html.

  2. R. Garrett, D. Cookson, G. Foran, T. Sabine, B. Kennedy, and S. Wilkins, Rev. Sci. Instrum. 66, 1351 (1995).

    Article  ADS  Google Scholar 

  3. A. N. Artemiev, A. D. Belyaev, N. A. Artemiev, A. A. Demkiv, A. G. Maevsky, O. Yu. Gorobtsov, B. F. Kirillov, S. I. Tyutyunnikov, and V. N. Shalyapin, “Debye-Scherrer diffraction in the backscattering geometry at the Kurchatov synchrotron radiation source. Part 1. Characterization of the method,” J. Surf. Invest.: X-ray, Synchrotr. Neutron Tech. 7, 916–920 (2013).

    Article  Google Scholar 

  4. A. N. Artemiev, A. D. Belyaev, N. A. Artemiev, A. A. Demkiv, A. G. Maevsky, O. Yu. Gorobtsov, B. F. Kirillov, G. A. Knyazev, S. I. Tyutyunnikov, and V. N. Shalyapin, “Debye-scherrer diffraction in the backscattering geometry at the Kurchatov synchrotron radiation source: Part 2. Equipment, pilot experiments and data processing,” J. Surf. Invest.: X-ray, Synchrotr. Neutron Tech. 8, 374–379 (2014).

    Article  Google Scholar 

  5. V. L. Aksenov, L. Gyngazov, I. Ivanov, S. I. Jeludeva, M. V. Kovalchiuk, M. Kovalenko, V. Minashkin, N. Scintee, V. N. Shaliapin, V. Skadorov, and S. I. Tiutiunnikov, “Universal energy-dispersive EXAFS spectrometer on the SR beam at the ‘Kurchatov Institute’ National Center,” Nucl. Instrum. Methods Phys. Res. A 448, 122–125 (2000).

    Article  ADS  Google Scholar 

  6. S. I. Tyutyunnikov, V. N. Shalyapin, V. L. Aksenov, A. N. Artem’ev, A. V. Zabelin, B. F. Kirillov, M. V.Koval’chuk, A. G. Maevskii, A. D. Belyaev, A. Porokhova, and V. A. Rezvov, “Physical startup of energy dispersive EXAFS spectrometer at kurchatov center of synchrotron radiation and nanotechnologies,” Phys. Part. Nucl. Lett. 6, 483–487 (2009).

    Article  Google Scholar 

  7. Fujifilm BAS-IP MS 2025 and Fujifilm BAS-IP SR 2025 (20 × 25 cm).

  8. www.esrf.eu/computing/scientific/FIT2D/fit2d_abstract. html.

  9. www.icdd.com.

  10. International Tables of X-ray Crystallography, Ed. by K. Lonsdale (Kynoch Press, Witton, Birmingham, UK, 1962), Vol. 3, pp. 162–195.

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Correspondence to V. N. Shalyapin.

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Original Russian Text © S.I. Tyutyunnikov, V.N. Shalyapin, A.D. Belyaev, A.N. Artemiev, N.A. Artemiev, B.F. Kirillov, M.V. Kovalchiuk, A.A. Demkiv, G.A. Knyazev, 2017, published in Pis’ma v Zhurnal Fizika Elementarnykh Chastits i Atomnogo Yadra, 2017.

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Tyutyunnikov, S.I., Shalyapin, V.N., Belyaev, A.D. et al. Multipurpose synchrotron spectrometer of the Kurchatov Institute: Part 3. Diffraction in Debye–Scherrer geometry. Phys. Part. Nuclei Lett. 14, 719–725 (2017). https://doi.org/10.1134/S1547477117050119

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  • DOI: https://doi.org/10.1134/S1547477117050119

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