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Effect of Xerogel and Powder Synthesis Conditions on the Properties of Ceramics Based on t-ZrO2 in the ZrO2–СeO2–Al2O3 System

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Abstract

Xerogels and powders of a solid solution based on zirconium dioxide are synthesized by the method of coprecipitation of hydroxides from aqueous solutions of salts of zirconium nitrate ZrO(NO3)2⋅2H2O, aluminum Al(NO3)3⋅9H2O, and cerium Ce(NO3)3⋅9H2O with an aqueous 1 M solution of ammonia NH4OH. A dense ceramic with low porosity and water absorption is obtained. The effect of the ultrasonic treatment of the precipitate and mechanical treatment of the xerogel on the physicochemical properties of the obtained materials is evaluated.

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Funding

This study was supported by the Russian Ministry of Education and Science as part of state assignment 0081-2022-0006 of the Institute of Silicate Chemistry, Russian Academy of Sciences.

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Authors and Affiliations

  1. Grebenshchikov Institute of Silicate Chemistry, Russian Academy of Sciences, 199034, St. Petersburg, Russia

    O. L. Belousova, A. N. Parunova, N. Yu. Fedorenko, V. L. Ugolkov, T. V. Khamova & O. A. Shilova

  2. St. Petersburg State Technological Institute (Technical University), 190013, St. Petersburg, Russia

    A. N. Parunova & O. A. Shilova

  3. St. Petersburg State Electrotechnical University “LETI, 197376, St. Petersburg, Russia

    O. A. Shilova

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  1. O. L. Belousova
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  2. A. N. Parunova
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  3. N. Yu. Fedorenko
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  4. V. L. Ugolkov
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  5. T. V. Khamova
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  6. O. A. Shilova
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Correspondence to O. L. Belousova.

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Belousova, O.L., Parunova, A.N., Fedorenko, N.Y. et al. Effect of Xerogel and Powder Synthesis Conditions on the Properties of Ceramics Based on t-ZrO2 in the ZrO2–СeO2–Al2O3 System. Glass Phys Chem 49, 664–671 (2023). https://doi.org/10.1134/S1087659623600667

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